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NMR Spectroscopy

NMR Solvents / Biomolecular NMR / NMR Tubes
Spectral Viewer / Synthesis / Reference Books
Spectroscopy Home

NMR Solvents

Deuterated NMR Solvents / High Purity Solvents
NMR Reference Standards / LC-NMR Reference Standards / LC-NMR solvents


Deuterated NMR Solvents

Aldrich and Isotec have shared manufacturing methods to offer a complete line of products for the NMR industry. We continually look for ways to improve our manufacturing process so we can offer you the best NMR solvent quality possible. Take a look at these NMR solvents that now have higher isotopic enrichment.

 

Cat. No. Product Information Unit Sizes
Chloroform-d (previous isotopic purity 99.8 atom % D)
15,182-3 Chloroform-d, 99.9 atom % D screw-cap 50g
    screw-cap 100g
    Sure/Seal™ 150g
    screw-cap 250g
23,689-6 Chloroform-d, 99.9 atom % D ampule 10 x 1.0mL
44,133-3 Chloroform-d, 99.9 atom % D ampule 10 x 0.75mL
52,201-5 Chloroform-d, 99.9 atom % D ampule 10 x 0.60mL
30,873-0 Chloroform-d, 99.9 atom % D ampule 5 x 0.5mL
22,578-9 Chloroform-d, 99.9 atom % D (contains 0.03% TMS) screw-cap 100g
    Sure/Seal™ 150g
    screw-cap 500g
42,366-1 Chloroform-d, 99.9 atom % D (contains 0.03% v/v TMS) ampule 10 x 1.0mL
15,183-1 Chloroform-d, 99.9 atom % D (contains 1% v/v TMS) screw-cap 50g
    screw-cap 100g
    Sure/Seal™ 150g
    screw-cap 250g
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Dichloromethane-d2 (previous isotopic purity 99.8 atom % D)
44,432-4 Dichloromethane-d2, 99.9 atom % D ampule 5g
    screw-cap 10g
    screw-cap 25g
44,610-6 Dichloromethane-d2, 99.9 atom % D ampule 10 x 0.75mL
52,203-1 Dichloromethane-d2, 99.9 atom % D ampule 10 x 0.6mL
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NEW High Purity Solvents

Aldrich now offers high purity NMR solvents that have minimum isotopic purity levels of 99.996 atom % D or better. These solvents offer the highest isotopic enrichment available for NMR applications where purity is absolutely crucial.

Cat. No. Product Information Unit Sizes
EXTRA (minimum 99.996 atom % D)
56,853-8 Chloroform-d , EXTRA ampule 10 x 0.75mL
61,339-8 Deuterium oxide, EXTRA Sure/Seal™ 10g
    ampule 50g
61,230-8 (Methyl sulfoxide)-d6, EXTRA ampule 10 x 0.25mL
    ampule 10 x 0.50mL
    ampule 10 x 0.75mL
 
ULTRA-D (minimum 99.999 atom % D)
61,340-1 Deuterium oxide, ULTRA-D ampule 10g
57,023-0 Deuterium oxide, ULTRA-D ampule 10 x 0.75mL
 
Improved DMSO-d6 Now Lower water
We have taken steps to improve the water levels in all of our DMSO listings. Order some today and experience the difference. We have also recently added DMSO-d6, 99.9 atom % D, “Special HOH”. D2O and HOD levels are kept to a minimum to avoid deuterium exchange with easily exchangeable protons in your sample.
61,232-4 (Methyl sulfoxide)-d6, 99.9 atom % D Special screw-cap 5g
  HOH screw-cap 25g
    screw-cap 50g
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NMR Reference Standards

We offer an extensive list of NMR reference standards in a variety of tube lengths. If there is a special mix you are interested in that we do not offer, please contact our Technical Services department at 800-231-8327(USA), or your local Sigma-Aldrich sales office.

Cat. No. Product Information Tube Size
61,177-8 1% Chloroform in acetone-d6, 99.9 atom % D 3mm x 8in
61,303-7 1% Chloroform in acetone-d6, 99.9 atom % D 4mm x 8in
61,177-8 1% Chloroform in acetone-d6, 99.9 atom % D 3mm x 8in
61,303-7 1% Chloroform in acetone-d6, 99.9 atom % D 4mm x 8in
61,174-3 1% Chloroform in acetone-d6, 99.9 atom % D 10mm x 8in
61,330-4 2% Chloroform in chloroform-d, 99.9 atom % D 3mm x 8in
61,331-2 2% Chlorform in chloroform-d, 99.9 atom % D 5mm x 8in
61,178-6 5% Chloroform in acetone-d6, 99.9 atom % D 3mm x 8in
61,183-2 5% Chloroform in acetone-d6, 99.9 atom % D 4mm Nano tube
61,185-9 20% Chloroform in acetone-d6, 99.8 atom % D 5mm x 8in
61,183-2 5% Chloroform in acetone-d6, 99.9 atom % D 4mm Nano tube
61,185-9 20% Chloroform in acetone-d6, 99.8 atom % D 5mm x 8in
61,251-0 5% 1,2-Dichlorobenzene in acetone-d6, 99.9 atom % D 5mm x 8in
61,211-1 40% 1,4-Dioxane in benzene-d6, 99.6 atom % D 3mm x 8in
61,179-4 40% 1,4-Dioxane in benzene-d6, 99.6 atom % D 4mm Nano tube
61,207-3 40% 1,4-Dioxane and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D 3mm x 8in
61,190-5 40% 1,4-Dioxane and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D 5mm x 8in
61,182-4 40% 1,4-Dioxane, and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D 4mm Nano tube
61,304-5 0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D 4mm x 8in
61,026-5 0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D 10mm x 8in
61,180-8 0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D 4mm Nano tube
61,248-0 0.1% Ethylbenzene, 0.01% TMS and 0.1mg/mL chromium(III) acetylacetonate in chloroform-d, 99.9 atom % D 5mm x 8in
61,293-6 5% Ethylbenzene and 2% TMS in chlorform-d, 99.9 atom % D 5mm x 7in
61,270-7 45% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D 3mm x 8in
61,189-1 45% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D 5mm x 8in
61,333-9 90% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D 3mm x 8in
61,208-1 0.1mg/mL Gadolinium(III) chloride, 0.1% DSS and 1% water in deuterium oxide, 99.9 atom % D 3mm x 8in
61,194-8 0.1mg/mL Gadolinium(III) chloride, 0.1% DSS and 1% water in deuterium oxide, 99.9 atom % D 8mm x 8in
61,181-6 0.1mg/mL Gadolinium(III) chloride in deuterium oxide, 99.9 atom % D 4mm Nano tube
61,192-1 25% Hexamethyldisiloxane in benzene-d6, 99.6 atom % D 5mm x 8in
61,329-0 50% Menthol and 0.5% chromium(III) acetylacetonate in chloroform-d, 99.9 atom % D 5mm x 8in
61,216-2 85% Phosphoric acid in deuterium oxide, 99.9 atom % D 5mm x 8in coaxial tube
61,191-3 0.2M Potassium fluoride and 90% water in deuterium oxide, 99.9 atom % D 10mm x 8in
61,268-5 0.05% a,a,a-Trifluorotoluene in benzene-d6, 99.6 atom % D 3mm x 8in
61,318-5 0.05% a,a,a-Trifluorotoluene in benzene-d6, 99.6 atom % D 4mm x 8in
61,117-9 0.0485M Triphenylphosphate in chlorform-d, 99.9 atom % D 8mm x 8in
61,173-5 0.0485M Triphenylphosphate in chloroform-d, 99.9 atom % D 10mm x 8in
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LC-NMR Reference Standards

Cat. No. Product Information Unit Size
61,244-8 1% Chloroform in acetone-d6, 99.9 atom % D screw-cap 50mL
61,302-9 50mM Sodium acetate and 1% water in deuterium oxide, 99.9 atom % D screw-cap 50mL
61,242-1 1% Water in deuterium oxide, 99.9 atom % D screw-cap 250mL
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LC-NMR Solvents

Cat. No. Product Information Unit Size
53,089-1 1% Chloroform in acetone-d6, 99.9 atom % D screw-cap 50mL
61,302-9 Acetone-d6, 99.5 atom % D GL-45 bottle 1L
53,088-3 Acetonitrile-d3, 99.8 atom % D GL-45 bottle 1L
56,310-2 Acetonitrile-d3, 99.8 atom % D (contains 15-20% D2O) GL-45 bottle 1L
53,086-7 Deuterium oxide, 99.9 atom % D GL-45 bottle 1L
53,087-5 Methyl-d3 alcohol-d, 99.8+ atom % D GL-45 bottle 1L
34955 Acetonitrile NMR CHROMASOLV® GL-45 bottle 500mL
      6 x 500mL
      1L
      6 x 1L
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