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Case Study Featured in Issue 20.2
Multi-Bed Adsorbent Tube Provides Better Results
red boxThe Problem
A customer who was interested in sampling for methylene chloride in an indoor air quality application called our Technical Service department recently. To determine what adsorbent tube would be required, we asked the customer what other compounds could be included in the sample. We learned that he was going to do the sampling in an environment that contained aromatic hydrocarbons (BTEX) in addition to methylene chloride.
The customer inquired about a thermal desorption tube to do this analysis. He was interested in a TDU tube that would be packed with a single bed of Carboxen-1000 material to do the analysis. He knew from published literature that this material would trap organic compounds with carbon chain lengths in the C2-C5 range.

The Solution
Our Technical Service representative informed the customer that the Carboxen-1000 custom TDU tube would not be a good choice for the analysis. Some of the BTEX compounds could be too strongly retained on the Carboxen-1000 material.
He suggested that the customer use our Carbotrap 317 TDU tubes which contains three adsorbent beds: Carbopack C, Carbopack B, and Carboxen-1000. The Carbopack C will trap organic compounds with carbon chain lengths in the C12-C20 range. The Carbopack B will trap compounds in the C5-C12 range. The Carboxen-1000 will trap compounds in the C2-C5 range. The first two beds will retain the BTEX compounds and serve to protect the bed of Carboxen-1000 material, which will collect the methylene chloride.
By using a multiple adsorbent bed tube, the customer was able to isolate the target compound of interest and effectively deal with the interfering aromatic hydrocarbons.
 
For more information, see
  T402025 (1,817 KB) "A Tool for Selecting an Adsorbent for Thermal Desorption Applications"
Other information related to this article:
Main Article Performance Tip Case Study   New Products Literature
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