52578-U Supelco

Supelclean PSA SPE Tube

bed wt. 200 mg, volume size 3 mL, pk of 54

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Properties

Related Categories Analytical/Chromatography, Sample Preparation & Purification, Solid Phase Extraction (SPE), Supelclean ENVI and Supelclean SPE Cartridges, Supelclean PSA SPE Products More...
material   PE frit (20 μm porosity)
  polypropylene hardware
composition   bed wt., 200 mg
packaging   pk of 54
extent of labeling   8.4% C loading
  3.3% N loading
volume size   3 mL
surface coverage   surface coverage 2.35 μmol/m2
matrix   silica gel base material (irregularly shaped)
matrix active group   ethylenediamine-N-propy bonding, polymerically bonded
particle size   50 μm
pore size   70 Å pore size
surface area   500 m2/g
pKa    (1) 10.1, (2) 10.9
capacity   0.98-1.05 meq/g capacity

Description

General description

Retention Mechanism: Normal-phase and anion-exchange
Sample Matrix Compatibility: Organic or aqueous solutions

• Polymerically bonded, ethylenediamine-N-propyl phase that contains both primary and secondary amines
• A weak anion exchanger with a pKa of 10.1 and 10.9
• Similar to aminopropyl SPE phases (NH2) in terms of selectivity, but has a much higher capacity due to presence of secondary amine (0.98-1.05 meq/g)
• Strong affinity and high capacity for removing fatty acids, organic acids, and some polar pigments and sugars when conducting multi-residue pesticide analysis in foods
• Has been shown to significantly reduce matrix-enhancement effects encountered during the GC analysis of food products
• Tested for superior cleanliness using GC-FID and GC-MS
• Bidentate nature of ligand allows for chelation

Legal Information

Supelclean is a trademark of Sigma-Aldrich Co. LLC

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