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183660 Aldrich

3,3-Dimethylacryloyl chloride

97%, contains 400 ppm phenothiazine as inhibitor

Synonym: 3-Methyl-2-butenoyl chloride, 3-Methylcrotonoyl chloride, Senecioyl chloride

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Properties

Related Categories Acid Halides, Building Blocks, Carbonyl Compounds, Chemical Synthesis, Organic Building Blocks More...
InChI Key   BDUBTLFQHNYXPC-UHFFFAOYSA-N
assay   97%
contains   400 ppm phenothiazine as inhibitor
refractive index   n20/D 1.476(lit.)
bp   145-147 °C(lit.)
density   1.065 g/mL at 25 °C(lit.)

Description

Packaging

5, 25 g in glass bottle

Application

3,3-Dimethylacryloyl chloride was used in the synthesis of:
• substituted 4,4-dimethyl-3,4-dihydro-1H-quinolin-2-one via condensation with aniline
• N-(3,3-Dimethylacryloyl)-(S)-leucine methyl ester

General description

3,3-Dimethylacryloyl chloride reacts with silylketene acetals in acetonitrile to give δ-ethylenic β-keto esters.

Price and Availability

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
Supplemental Hazard Statements 
Reacts violently with water.
RIDADR 
UN 2920 3(8) / PGII
WGK Germany 
3
Flash Point(F) 
123.8 °F
Flash Point(C) 
51 °C
Protocols & Articles
Peer-Reviewed Papers
15

References

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