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238112 Aldrich

1,2-Diiodobenzene

98%

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Properties

Related Categories Aryl, Building Blocks, C6, Chemical Synthesis, Halogenated Hydrocarbons,
assay   98%
refractive index   n20/D 1.718(lit.)
bp   152 °C/15 mmHg(lit.)
density   2.524 g/mL at 25 °C(lit.)
storage temp.   2-8°C

Description

Packaging

1, 10 g in glass bottle

Application

1,2-Diiodobenzene has been used in the preparation of purino[8,9-f]phenanthridines1.

General description

Photolysis of 1,2-diiodobenzene in cyclohexane, furan, benzene and benzene containing tetraphenylcyclopentadienone has been studied2.

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Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
WGK Germany 
3
Flash Point(F) 
235.4 °F
Flash Point(C) 
113 °C

Protocols & Articles

Peer-Reviewed Papers

References

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1. Intramolecular direct C-H arylation approach to fused purines. Synthesis of purino[8,9-f]phenanthridines and 5,6-dihydropurino[8,9-a]isoquinolines. Cerna I, Pohl R, Klepetárová B, et al. J. Org. Chem. 75(7), 2302-8, (2010)

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2. The Photolysis of 1, 2-Diiodobenzene: A Photochemical Source of Benzyne. Kampmeier JA and Hoffmeister E. J. Am. Chem. Soc. 84(19), 3787-88, (1962)

Beil. 5,225

Aldrich MSDS 1, 713:A / Corp MSDS 1 (1), 1283:D / FT-IR 1 (1), 978:B / FT-IR 2 (2), 1688:B / FT-NMR 1 (2), 71:A / RegBook 1 (1), 1169:J / Structure Index 1, 179:E:7 / Vapor Phase 3, 895:C

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