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269131 Aldrich

2-(2-Bromoethyl)-1,3-dioxane

98%

Synonym: 3-Bromopropionaldehyde trimethylene acetal

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Properties

Related Categories Acetals/Ketals/Ortho Esters, Building Blocks, Chemical Synthesis, Organic Building Blocks, Oxygen Compounds More...
InChI Key   WMDHQEHPOVOEOG-UHFFFAOYSA-N
assay   98%
refractive index   n20/D 1.481(lit.)
bp   67-70 °C/2.8 mmHg(lit.)
solubility   ethanol: soluble50 (μg/mL)
density   1.431 g/mL at 25 °C(lit.)

Description

Packaging

10, 50 g in glass bottle

Application

2-(2-Bromoethyl)-1,3-dioxane was used in the synthesis of ketone adducts 2-[3-oxo-4(S)-(triphenylmethyl) amino-6-methylheptyl]-1,3-dioxane and 2-[3-oxo-4(S)-(triphenylmethyl)amino-6-methylheptyl]-1,3-dioxolane.

General description

The reaction of Grignard reagent prepared from 2-(2-bromoethyl)-1,3-dioxane and N-tert-butanesulfinyl aldimines was studied.

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Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
RIDADR 
NONH for all modes of transport
WGK Germany 
3
Flash Point(F) 
206.6 °F
Flash Point(C) 
97 °C
Protocols & Articles
Peer-Reviewed Papers
15

References

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