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274879 Aldrich

1,4-Cyclohexanedione monoethylene acetal

97%

Synonym: 1,4-Dioxaspiro[4.5]decan-8-one

  • CAS Number 4746-97-8

  • Empirical Formula (Hill Notation) C8H12O3

  • Molecular Weight 156.18

  •  Beilstein Registry Number 117631

  •  MDL number MFCD00010214

  •  PubChem Substance ID 24856612

  • Popular Documents:  FTNMR (PDF)  

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Properties

Related Categories Acetals/Ketals/Ortho Esters, Building Blocks, Chemical Synthesis, Organic Building Blocks, Oxygen Compounds More...
assay   97%
mp   70-73 °C(lit.)

Description

Application

Used in a study of microwave-assisted reductive amination.1

Via a novel aromatization process, this bicyclic frame can be converted into a series of 5-alkoxytryptamine derivatives including serotonin, melatonin and bufotenin

Packaging

5, 25, 100 g in glass bottle

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Safety & Documentation

Safety Information

WGK Germany 
3

Documents

Certificate of Analysis

Certificate of Origin

Protocols & Articles

Peer-Reviewed Papers

References

Set your institution to view full text papers.

1. Synlett, 2444, (2006)

Aldrichimica Acta 12, 40, (1979)

Tetrahedron 50, 731, (1994)

Synlett, 81, (1994)

Synth. Commun. 24, 799, (1994)

Tetrahedron Lett. 45, 4859, (2004)

Tetrahedron Lett. 45, 4661, (2004)

A mild method for the preparation of gamma-hydroxy-alpha,beta-acetylenic esters. Angew. Chem. Int. Ed. Engl. 43, 2525, (2004)

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Aromatization of 1,6,7,7a-tetrahydro-2H-indol-2-ones by a novel process. Preparation of key-intermediate methyl 1-benzyl-5-methoxy-1H-indole-3-acetate and the syntheses of serotonin, melatonin, and bufotenin. Revial, G.; et al. J. Org. Chem. 67, 2252, (2002)

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Beil. 19,V,4,93

FT-NMR 1 (1), 722:C / RegBook 1 (1), 501:D / Structure Index 1, 72:A:1

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