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274879 Aldrich

1,4-Cyclohexanedione monoethylene acetal

97%

Synonym: 1,4-Dioxaspiro[4.5]decan-8-one

  • CAS Number 4746-97-8

  • Empirical Formula (Hill Notation) C8H12O3

  • Molecular Weight 156.18

  •  Beilstein Registry Number 117631

  •  MDL number MFCD00010214

  •  PubChem Substance ID 24856612

  • Popular Documents:  FTNMR (PDF)  

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Properties

Related Categories Acetals/Ketals/Ortho Esters, Building Blocks, Chemical Synthesis, Organic Building Blocks, Oxygen Compounds More...
assay   97%
mp   70-73 °C(lit.)

Description

Application

Used in a study of microwave-assisted reductive amination.1

Via a novel aromatization process, this bicyclic frame can be converted into a series of 5-alkoxytryptamine derivatives including serotonin, melatonin and bufotenin

Packaging

5, 25, 100 g in glass bottle

Price and Availability

Safety & Documentation

Safety Information

WGK Germany 
3

Documents

Certificate of Analysis

Certificate of Origin

Protocols & Articles

Peer-Reviewed Papers

References

Set your institution to view full text papers.

1. Synlett, 2444, (2006)

A mild method for the preparation of gamma-hydroxy-alpha,beta-acetylenic esters. Angew. Chem. Int. Ed. Engl. 43, 2525, (2004)

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Aldrichimica Acta 12, 40, (1979)

Tetrahedron 50, 731, (1994)

Synlett, 81, (1994)

Synth. Commun. 24, 799, (1994)

Tetrahedron Lett. 45, 4859, (2004)

Tetrahedron Lett. 45, 4661, (2004)

Aromatization of 1,6,7,7a-tetrahydro-2H-indol-2-ones by a novel process. Preparation of key-intermediate methyl 1-benzyl-5-methoxy-1H-indole-3-acetate and the syntheses of serotonin, melatonin, and bufotenin. Revial, G.; et al. J. Org. Chem. 67, 2252, (2002)

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Beil. 19,V,4,93

FT-NMR 1 (1), 722:C / RegBook 1 (1), 501:D / Structure Index 1, 72:A:1

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