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452556 Aldrich

Ethanol-OD

99 atom % D

Synonym: Ethan(ol-d), Ethyl alcohol-OD

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Properties

Related Categories Additional NMR Solvents, Alphabetical Listings, E-F, NMR Solvents, NMR Solvents and Reagents,
InChI Key   LFQSCWFLJHTTHZ-WFVSFCRTSA-N
isotopic purity   99 atom % D
assay   99% (CP)
refractive index   n20/D 1.359(lit.)
bp   78 °C(lit.)
mp   -114 °C(lit.)
density   0.806 g/mL at 25 °C
mass shift   M+1

Description

Packaging

25, 100 mL in glass bottle

Application

Ethan(ol-d) may be used as a source of deuterium for the deuterium exchange reaction of ethyl acetoacetate.

General description

Ethan(ol-d) (ethanol-d, ethanol-d1) is a deuterated NMR solvent useful in NMR-based research and analyses. It can be prepared by reacting tetraethylorthosilicate with deuterium oxide. The hydrogen bonding in ethanol-d1 has been investigated based on Raman spectral data. The far infrared (FIR) spectrum of ethanol-d1 has been studied using ab initio calculations.

Price and Availability


Stable Isotope
Safety & Documentation

Safety Information

Symbol 
GHS02  GHS02
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN1170 - class 3 - PG 2 - Ethanol
WGK Germany 
1
Flash Point(F) 
57.2 °F
Flash Point(C) 
14 °C
Protocols & Articles

Related Content

Properties of Solvents Table

a. Gant, R., LC/GC 10(7), 515 (1992) 1. At 20 °C 2. At 20 °C +/- 5 °C relative to water at 4 °C 3. At 10mmHg pressure 4. At l=589.32nm
Keywords: Gas chromatography, High performance liquid chromatography

Peer-Reviewed Papers
15

References

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