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471623 Aldrich

1,1,1-Trimethylhydrazinium iodide

97%

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Properties

Related Categories Building Blocks, Chemical Synthesis, Hydrazines, Nitrogen Compounds, Organic Building Blocks More...
InChI Key   HLNPDVKKRBWQAA-UHFFFAOYSA-M
assay   97%
mp   225-230 °C (dec.)(lit.)

Description

Packaging

50 g in glass bottle

Application

1,1,1-Trimethylhydrazinium iodide (TMHI) may be employed for the amination of 1-X-3,5-dinitrobenzenes.

General description

1,1,1-Trimethylhydrazinium iodide ([(CH3)3N-NH2]I, TMHI) is widely employed as a vicarious nucleophilic substitution (VNS) reagent for various aromatic amination reactions. On reaction with silver salt, it affords the following salts: nitrate (([(CH3)3N-NH2][NO3]), perchlorate ([(CH3)3N-NH2][ClO4]), azide ([(CH3)3N-NH2][N3]), 5-amino-1H-tetrazolate ([(CH3)3N-NH2][H2N-CN4]) and sulfate ([(CH3)3N-NH2]2[SO4].2H2O).

Price and Availability

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
Personal Protective Equipment 
RIDADR 
NONH for all modes of transport
WGK Germany 
3
RTECS 
MW0349100
Protocols & Articles
Peer-Reviewed Papers
15

References

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