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494976 Aldrich

3-Bromothianaphthene

95%

Synonym: 3-Bromobenzo[b]thiophene

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Properties

Related Categories Benzothiophenes, Building Blocks, Chemical Synthesis, Halogenated Heterocycles, Heterocyclic Building Blocks More...
InChI Key   SRWDQSRTOOMPMO-UHFFFAOYSA-N
assay   95%
refractive index   n20/D 1.668(lit.)
bp   269 °C/752.5 mmHg(lit.)
density   1.629 g/mL at 25 °C(lit.)

Description

Packaging

5, 25 mL in glass bottle

Application

3-Bromothianaphthene may be used in the synthesis of (benzo[b]thiophen-3-yl)trimethylstannane.

General description

3-Bromothianaphthene is a heteroaryl halide. It undergoes Suzuki-Miyaura reaction with phenylboronic acid (PBA) or 3-thienylboronic acid in the presence of a novel heterogeneous Pd catalyst [Pd@PDEB, PDEB=poly(1,3-diethynylbenzene)]. The substitution reaction of 3-bromothianaphthene with piperidine to form 3-piperidinothianaphthene as the major product has been reported.

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Safety & Documentation

Safety Information

RIDADR 
NONH for all modes of transport
WGK Germany 
3
Flash Point(F) 
>235.4 °F
Flash Point(C) 
>113 °C

Documents

Certificate of Analysis

Certificate of Origin

Protocols & Articles
Peer-Reviewed Papers
15

References

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