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511382 Aldrich

1-Boc-hexahydro-1,4-diazepine

98%

Synonym: 1-Boc-homopiperazine, tert-Butyl homopiperazine-1-carboxylate

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Properties

Related Categories Building Blocks, C10, Chemical Synthesis, Heterocyclic Building Blocks, Piperazines More...
InChI Key   WDPWEXWMQDRXAL-UHFFFAOYSA-N
assay   98%
refractive index   n20/D 1.471(lit.)
bp   95-110 °C/0.5 mmHg(lit.)
density   1.016 g/mL at 20 °C(lit.)

Description

Application

Used in synthesis of potent anticoagulant.

Packaging

5 g in glass bottle

General description

1-Boc-hexahydro-1,4-diazepine is an N-boc protected homopiperazine. Its enthalpy of vaporization at boiling point (558.15K) is 49.498kjoule/mol.

Price and Availability

Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
RIDADR 
NONH for all modes of transport
WGK Germany 
3
Flash Point(F) 
230 °F
Flash Point(C) 
110 °C
Protocols & Articles

Articles

MRT - Ring Expansion

Potentially hazardous reagents like diazo compounds can be handled safely in microreactors because actual reaction volumes are very small. In a procedure developed at Johnson&Johnson ethyl diazoaceta...
Matthias Junkers
Aldrich ChemFiles 2009, 9.4, 13.
Keywords: Catalog, Chemfiles, Condensations, Continuous flow chemistry, Decarboxylations, Dieckmann Condensation, Michael Addition, Microreactor technology, Ring expansion

Peer-Reviewed Papers
15

References

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