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530735 Aldrich

Chloroform-d

≥99.8 atom % D, contains 0.5 wt. % silver foil as stabilizer, 0.03 % (v/v) TMS

Synonym: Deuterochloroform

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Properties

Related Categories Alphabetical Listings, C, Chloroform, Chloroform-d, NMR Solvents,
InChI Key   HEDRZPFGACZZDS-MICDWDOJSA-N
isotopic purity   ≥99.8 atom % D
assay   ≥99% (CP)
contains   0.5 wt. % silver foil as stabilizer
  0.03 % (v/v) TMS
refractive index   n20/D 1.444(lit.)
bp   60.9 °C(lit.)
mp   −64 °C(lit.)
density   1.500 g/mL at 25 °C(lit.)
mass shift   M+1

Description

Packaging

100, 250 g in glass bottle

Application

Chloroform-d may be used in the synthesis of dichlorofluoromethane-d.

General description

Chloroform-d (deuterochloroform, CDCl3) is a deuterated NMR solvent containing 0.03% (v/v) TMS (tetramethylsilane) and 0.5wt.% silver foil as stabilizer. It is useful in NMR-based research and analyses. It may be synthesized by reacting trichloroacetophenone and sodium deuteroxide. The influence of the number of pulses on its multiphoton decomposition (MPD) has been studied. Infrared spectral studies of C-D stretching and bending motions of CDCl3 in different solvents have been investigated. The effect of chloroform-d on the interaction of water with activated carbons has been analyzed. The dependence of molecular reorientation of deuterated chloroform on pressure and temperature has been studied by Raman spectroscopy.

Price and Availability


Stable Isotope
Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
RIDADR 
UN 1888 6.1 / PGIII
WGK Germany 
3
Protocols & Articles
Peer-Reviewed Papers
15

References

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