Aldrich® sublimation apparatus
capacity, ≤ 3 g starting material
DOWNLOAD MSDS (PDF)
Properties
| Related Categories | Aldrich, Aldrich Sublimation, Aldrich sublimation apparatus and accessories, Glass Sublimation Supplies, Glassware, |
| feature | capacity≤ 3 g starting material |
Description
General description
With reversed, screw-thread ST joint and 2 mm glass stopcock. O-ring seals joint without grease, thus eliminating contamination when removing sublimator head. Flat-bottom on inner tube for easy sample removal.
Operation:
1. Place material to be sublimated in bottom of lower vessel
2. Attach condenser assembly to the lower vessel and tighten red cap nut
3. Connect coolant supply hose to upper hose connector and coolant return hose to lower connector
4. Connect vacuum source to stopcock hose connection
5. Place lower vessel into heating mantle
6. Start flow of coolant through condenser assembly
7. Evacuate lower vessel
8. Turn on heating mantle
9. Sublimation begins
Components:
Z557072, Aldrich sublimation head, for Z221163
Z557056, Aldrich sublimation head, for Z221171
Z557080, Aldrich sublimation reservoir, for Z221163
Z557064, Aldrich sublimation reservoir, for Z221171
Legal Information
Aldrich is a registered trademark of Sigma-Aldrich Co. LLC
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