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77247 Fluka

Heptafluorobutyric acid

≥99.0% (GC)

Synonym: Edman Reagent No. 3, HFBA, Perfluorobutyric acid

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Properties

Related Categories Molecular Biology, Protein Sequencing, Protein Structural Analysis, Proteomics, Reagents for Protein Sequencing More...
vapor density   7 (vs air)
vapor pressure   ~10 mmHg ( 25 °C)
assay   ≥99.0% (GC)
refractive index   n20/D 1.3(lit.)
bp   120 °C/755 mmHg(lit.)
density   1.645 g/mL at 25 °C(lit.)

Description

Other Notes

This product has been replaced by 77249-SIGMA | Heptafluorobutyric acid ≥99.0% (GC)

Price and Availability

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Safety & Documentation

Safety Information

Symbol 
GHS05  GHS05
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN 3265 8 / PGI
WGK Germany 
3
RTECS 
ET4025000

Protocols & Articles

Peer-Reviewed Papers

References

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Distribution and sources of polyfluoroalkyl substances (PFAS) in the River Rhine watershed. Möller A, Ahrens L, Surm R, et al. Environ. Pollut. 158(10), 3243-50, (2010)

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Structure-activity relationship assessment of four perfluorinated chemicals using a prolonged zebrafish early life stage test. Hagenaars A, Vergauwen L, De Coen W, et al. Chemosphere 82(5), 764-72, (2011)

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Structural analysis of naturally occurring sialic acids. Kamerling JP and Gerwig GJ Methods Mol. Biol. 347, 69-91, (2006)

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Comparative pharmacokinetics of perfluorobutyrate in rats, mice, monkeys, and humans and relevance to human exposure via drinking water. Chang SC, Das K, Ehresman DJ, et al. Toxicol. Sci. 104(1), 40-53, (2008)

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Polyfluoroalkyl compounds in landfill leachates. Busch J, Ahrens L, Sturm R, et al. Environ. Pollut. 158(5), 1467-71, (2010)

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Accumulation of perfluoroalkyl substances in human tissues. Pérez F, Nadal M, Navarro-Ortega A, et al. Environ. Int. 59, 354-62, (2013)

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Light-induced degradation of perfluorocarboxylic acids in the presence of titanium dioxide. Dillert R, Bahnemann D, and Hidaka H Chemosphere 67(4), 785-92, (2007)

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Effects of perfluorobutyrate exposure during pregnancy in the mouse. Das KP, Grey BE, Zehr RD, et al. Toxicol. Sci. 105(1), 173-81, (2008)

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Analysis of perfluoroalkyl substances in waters from Germany and Spain. Llorca M, Farré M, Picó Y, et al. Sci. Total Environ. 431, 139-50, (2012)

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Behavior of perfluorinated compounds in soils during leaching experiments. Gellrich V, Stahl T, and Knepper TP Chemosphere 87(9), 1052-6, (2012)

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Application of perfluorinated acids as ion-pairing reagents for reversed-phase chromatography and retention-hydrophobicity relationships studies of selected beta-blockers. Flieger J J. Chromatogr. A 1217(4), 540-9, (2010)

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Analysis of underivatized polyamines by reversed phase liquid chromatography with electrospray tandem mass spectrometry. Häkkinen MR, Keinänen TA, Vepsäläinen J, et al. J. Pharm. Biomed. Anal. 45(4), 625-34, (2007)

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Perfluoroalkyl substances (PFASs) in food and water from Faroe Islands. Eriksson U, Kärrman A, Rotander A, et al. Environ. Sci. Pollut. Res. Int. 20(11), 7940-8, (2013)

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Separation of amaranthine-type betacyanins by ion-pair high-speed countercurrent chromatography. Jerz G, Gebers N, Szot D, et al. J. Chromatogr. A 1344, 42-50, (2014)

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Differential hepatic effects of perfluorobutyrate mediated by mouse and human PPAR-alpha. Foreman JE, Chang SC, Ehresman DJ, et al. Toxicol. Sci. 110(1), 204-11, (2009)

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Separation of polar betalain pigments from cacti fruits of Hylocereus polyrhizus by ion-pair high-speed countercurrent chromatography. Wybraniec S, Stalica P, Jerz G, et al. J. Chromatogr. A 1216(41), 6890-9, (2009)

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Simultaneous detection and quantitation of highly water-soluble herbicides in serum using ion-pair liquid chromatography-tandem mass spectrometry. Wang KC, Chen SM, Hsu JF, et al. J. Chromatogr. B. Analyt. Technol. Biomed. Life Sci. 876(2), 211-8, (2008)

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Toxicological evaluation of ammonium perfluorobutyrate in rats: twenty-eight-day and ninety-day oral gavage studies. Butenhoff JL, Bjork JA, Chang SC, et al. Reprod. Toxicol. 33(4), 513-30, (2012)

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Adsorption of four perfluorinated acids on non ion exchange polymer sorbents. Senevirathna ST, Tanaka S, Fujii S, et al. Water Sci. Technol. 63(10), 2106-13, (2011)

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Cooperative effect in ion pairing of oligolysine with heptafluorobutyric acid in reversed-phase chromatography. Xie W, Qin X, Teraoka I, et al. J. Chromatogr. A 1218(43), 7765-70, (2011)

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Simultaneous determination of flavonoid and alkaloid compounds in Citrus herbs by high-performance liquid chromatography-photodiode array detection-electrospray mass spectrometry. Ding L, Luo X, Tang F, et al. J. Chromatogr. B. Analyt. Technol. Biomed. Life Sci. 857(2), 202-9, (2007)

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Separation of Amadori peptides from their unmodified analogs by ion-pairing RP-HPLC with heptafluorobutyric acid as ion-pair reagent. Frolov A and Hoffmann R Anal. Bioanal. Chem 392(6), 1209-14, (2008)

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Solvolytic reactivity of heptafluorobutyrates and trifluoroacetates. Denegri B and Kronja O J. Org. Chem. 74(16), 5927-33, (2009)

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GC separation of amino acid enantiomers via derivatization with heptafluorobutyl chloroformate and Chirasil-L-Val column. Zahradnícková H, Husek P, and Simek P J. Sep. Sci. 32(22), 3919-24, (2009)

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Underivatized polyamine analysis in plant samples by ion pair LC coupled with electrospray tandem mass spectrometry. Sánchez-López J, Camañes G, Flors V, et al. Plant Physiol. Biochem. 47(7), 592-8, (2009)

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Preconcentration and decomposition of perfluorinated carboxylic acids on an activated charcoal cartridge with sodium biphenyl reagent and its determination at microg L(-1) level on the basis of flow injection-fluorimetric detection of fluoride ion. Takayanagi T, Yamashita H, Motomizu S, et al. Talanta 74(5), 1224-30, (2008)

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Quantitation of quinapril in human plasma by matrix-assisted laser desorption ionization time-of-flight mass spectrometry with quinolone matrix additives. Lu CY, Liu FT, and Feng CH J. Chromatogr. B. Analyt. Technol. Biomed. Life Sci. 879(26), 2688-94, (2011)

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Interconversion of ephedrine and pseudoephedrine during chemical derivatization. Wong CH, Ho EN, Kwok WH, et al. Drug Test. Anal. 4(12), 1028-33, (2012)

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Distribution and primary source analysis of per- and poly-fluoroalkyl substances with different chain lengths in surface and groundwater in two cities, North China. Yao Y, Zhu H, Li B, et al. Ecotoxicol. Environ. Saf. 108, 318-28, (2014)

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Beil. 2,IV,810

Aldrich MSDS 1, 1005:A / Corp MSDS 1 (1), 1819:A / FT-IR 2 (1), 796:D / FT-IR 1 (1), 507:A / FT-NMR 1 (1), 800:B / IR-Spectra (3), 297:E / IR-Spectra (2), 268:B / RegBook 1 (1), 559:J / Sax 6, 1498 / Sigma FT-IR 1 (2), 602:A / Structure Index 1, 79:D:7 / Vapor Phase 3, 590:A

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