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86042 Fluka

Sulfamic acid

≥99.0% (T)

Synonym: Amidosulfonic acid

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Properties

Related Categories Acids, Acids & Bases, Chemical Synthesis, Organic Acids, Synthetic Reagents More...
assay   ≥99.0% (T)
ign. residue   ≤0.1% (as SO4)
mp   215-225 °C (dec.)(lit.)
anion traces   chloride (Cl-): ≤50 mg/kg
  sulfate (SO42-): ≤500 mg/kg
cation traces   Ca: ≤50 mg/kg
  Cd: ≤50 mg/kg
  Co: ≤50 mg/kg
  Cu: ≤50 mg/kg
  Fe: ≤50 mg/kg
  K: ≤100 mg/kg
  Na: ≤100 mg/kg
  Ni: ≤50 mg/kg
  Pb: ≤50 mg/kg
  Zn: ≤50 mg/kg

Description

Other Notes

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Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
Personal Protective Equipment 
Hazard Codes (Europe) 
Xi
Risk Statements (Europe) 
Safety Statements (Europe) 
26-28-61
RIDADR 
UN 2967 8 / PGIII
WGK Germany 
1

Documents

Certificate of Analysis

Protocols & Articles

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Molarity Calculator and Normality Calculator for Acids and Bases

The molarity calculator tool provides lab-ready directions describing how to prepare an acid or base solution of specified Molarity (M) or Normality (N) from a concentrated acid or base solution.  To...

Peer-Reviewed Papers

References

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1. G.A. Benson, W.J. Spillane Chem. Rev. 80, 151, (1980)

Measurement of nitrosamine and nitramine formation from NOx reactions with amines during amine-based carbon dioxide capture for postcombustion carbon sequestration. Dai N, Shah AD, Hu L, et al. Environ. Sci. Technol. 46(17), 9793-801, (2012)

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Cobalt-catalyzed direct arylation and benzylation by C-H/C-O cleavage with sulfamates, carbamates, and phosphates. Song W and Ackermann L Angew. Chem. Int. Ed. Engl. 51(33), 8251-4, (2012)

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Nickel-catalyzed amination of aryl sulfamates and carbamates using an air-stable precatalyst. Hie L, Ramgren SD, Mesganaw T, et al. Org. Lett. 14(16), 4182-5, (2012)

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Comparison of arylboron-based nucleophiles in Ni-catalyzed Suzuki-Miyaura cross-coupling with aryl mesylates and sulfamates. Zhang N, Hoffman DJ, Gutsche N, et al. J. Org. Chem. 77(14), 5956-64, (2012)

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Modular functionalization of allenes to aminated stereotriads. Adams CS, Boralsky LA, Guzei IA, et al. J. Am. Chem. Soc. 134(26), 10807-10, (2012)

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Iron-catalyzed cross-coupling reactions of alkyl Grignards with aryl sulfamates and tosylates. Agrawal T and Cook SP Org. Lett. 15(1), 96-9, (2013)

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[(Cp-R)M(CO)3] (M=Re or 99mTc) Arylsulfonamide, arylsulfamide, and arylsulfamate conjugates for selective targeting of human carbonic anhydrase IX. Can D, Spingler B, Schmutz P, et al. Angew. Chem. Int. Ed. Engl. 51(14), 3354-7, (2012)

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Palladium-catalysed aminosulfonylation of aryl-, alkenyl- and heteroaryl halides: scope of the three-component synthesis of N-aminosulfonamides Emmett, E. J., et al. Org. Biomol. Chem. 10, 4007-4014, (2012)

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Palladium-catalyzed intramolecular diamination of acrylic esters using sulfamates as nitrogen source. Chávez P, Kirsch J, Streuff J, et al. J. Org. Chem. 77(4), 1922-30, (2012)

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Detection of the 1H and 15N NMR resonances of sulfamate groups in aqueous solution: a new tool for heparin and heparan sulfate characterization. Langeslay DJ, Beni S, and Larive CK Anal. Chem. 83(20), 8006-10, (2011)

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Sulfamate proton solvent exchange in heparin oligosaccharides: evidence for a persistent hydrogen bond in the antithrombin-binding pentasaccharide Arixtra. Langeslay DJ, Young RP, Beni S, et al. Glycobiology 22(9), 1173-82, (2012)

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Ureido-substituted sulfamates show potent carbonic anhydrase IX inhibitory and antiproliferative activities against breast cancer cell lines. Winum JY, Carta F, Ward C, et al. Bioorg. Med. Chem. Lett. 22(14), 4681-5, (2012)

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Cloning, characterization and sulfonamide inhibition studies of an ?-carbonic anhydrase from the living fossil sponge Astrosclera willeyana. Anna Ohradanova et al Bioorg. Med. Chem. 20, 1403-10, (2012)

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Promiscuity of carbonic anhydrase II. Unexpected ester hydrolysis of carbohydrate-based sulfamate inhibitors. Lopez M, Vu H, Wang CK, et al. J. Am. Chem. Soc. 133(45), 18452-62, (2011)

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Proton-in-flight mechanism for the spontaneous hydrolysis of N-methyl O-phenyl sulfamate: implications for the design of steroid sulfatase inhibitors. Edwards DR and Wolfenden R J. Org. Chem. 77(9), 4450-3, (2012)

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Hydrolysis of N-alkyl sulfamates and the catalytic efficiency of an S-N cleaving sulfamidase. Lohman DC, Wolfenden R, and Edwards DR J. Org. Chem. 77(6), 2907-10, (2012)

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Total synthesis of (-)-kaitocephalin based on a Rh-catalyzed C-H amination. Takahashi K, Yamaguchi D, Ishihara J, et al. Org. Lett. 14(6), 1644-7, (2012)

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QSAR studies of sulfamate and sulfamide inhibitors targeting human carbonic anhydrase isozymes I, II, IX and XII. Tarko L and Supuran CT Bioorg. Med. Chem. 21(6), 1404-9, (2013)

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Potent inhibition of Norwalk virus by cyclic sulfamide derivatives. Dou D, Tiew KC, He G, et al. Bioorg. Med. Chem. 19(20), 5975-83, (2011)

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Phosphine-catalyzed [3 + 2] cycloaddition of sulfamate-derived cyclic imines with allenoate: synthesis of sulfamate-fused dihydropyrroles. Yu H, Zhang L, Yang Z, et al. J. Org. Chem. 78(17), 8427-36, (2013)

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Glycosidic carbonic anhydrase IX inhibitors: a sweet approach against cancer. Winum JY, Colinas PA, and Supuran CT Bioorg. Med. Chem. 21(6), 1419-26, (2013)

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Mechanistic Studies of Substrate-assisted Inhibition of Ubiquitin-activating Enzyme by Adenosine Sulfamate Analogues. Chen, J.J., et al J. Biol. Chem. 286, 40867-40877, (2011)

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Acyl-sulfamates target the essential glycerol-phosphate acyltransferase (PlsY) in Gram-positive bacteria. Cherian PT, Yao J, Leonardi R, et al. Bioorg. Med. Chem. 20(16), 4985-94, (2012)

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A modular synthesis of dithiocarbamate pendant unnatural α-amino acids. Saha A, Baig RB, Leazer J, et al. Chem. Commun. (Camb.) 48(71), 8889-91, (2012)

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Efficacious N-protection of O-aryl sulfamates with 2,4-dimethoxybenzyl groups. Reuillon T, Bertoli A, Griffin RJ, et al. Org. Biomol. Chem. 10(37), 7610-7, (2012)

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Ethylenediammonium dication: H-bonded complexes with terephthalate, chloroacetate, phosphite, selenite and sulfamate anions. Detailed vibrational spectroscopic and theoretical studies of ethylenediammonium terephthalate. Marchewka MK and Drozd M Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 99, 223-33, (2012)

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Merck 14,8921

Fieser 1,1117

Aldrich MSDS 1, 1627:A / Corp MSDS 1 (2), 3196:C / FT-IR 2 (3), 4710:D / FT-IR 1 (2), 1231:A / RegBook 1 (3), 3199:D / Sax 6, 2479 / Sigma FT-IR 1 (2), 1048:D / Structure Index 1, 509:B:2

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86040 Sulfamic acid, analytical standard (for acidimetry), ACS reagent

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