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92330 Fluka

Trimethyl borate

purum, ≥99.0% (GC)

Synonym: Boric acid trimethyl ester, Methyl borate

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Properties

Related Categories Boronic Acids and Derivatives, Chemical Synthesis, Organoborates, Organometallic Reagents
vapor density   3.59 (vs air)
grade   purum
assay   ≥99.0% (GC)
refractive index   n20/D 1.346(lit.)
  n20/D 1.358
bp   68-69 °C(lit.)
mp   −34 °C(lit.)
density   0.932 g/mL at 20 °C(lit.)

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Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Target organs 
Central nervous system, Eyes
RIDADR 
UN 2416 3 / PGII
WGK Germany 
2
RTECS 
ED5600000
Flash Point(F) 
19.4 °F
Flash Point(C) 
-7 °C

Protocols & Articles

Peer-Reviewed Papers

References

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Gas phase reactions of trimethyl borate with phosphates and their non-covalent complexes. Gronert S and O'Hair RA J. Am. Soc. Mass Spectrom. 13(9), 1088-98, (2002)

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Identification of the carboxylic acid functionality by using electrospray ionization and ion-molecule reactions in a modified linear quadrupole ion trap mass spectrometer. Habicht SC, Vinueza NR, Archibold EF, et al. Anal. Chem. 80(9), 3416-21, (2008)

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Borinium adduct ion formation with barbiturates in a quadrupole ion-trap mass spectrometer. Colorado A and Brodbelt J J. Mass Spectrom. 31(4), 403-10, (1996)

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Identification of epoxide functionalities in protonated monofunctional analytes by using ion/molecule reactions and collision-activated dissociation in different ion trap tandem mass spectrometers. Eismin RJ, Fu M, Yem S, et al. J. Am. Soc. Mass Spectrom. 23(1), 12-22, (2012)

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11B magnetic resonance imaging and MAS spectroscopy of trimethylborate-treated radiata pine wood. Meder R, Franich RA, and Callaghan PT Solid State Nucl. Magn. Reson. 15(1), 69-72, (1999)

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Differentiation of protonated aromatic regioisomers related to lignin by reactions with trimethylborate in a Fourier transform ion cyclotron resonance mass spectrometer. Somuramasami J, Duan P, Amundson LM, et al. J. Am. Soc. Mass Spectrom. 22(6), 1040-51, (2011)

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Chloromethyl chlorosulfate: a new, catalytic method of preparation and reactions with some nucleophiles. Org. Biomol. Chem. 2, 1554, (2004)

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Merck 14,9712

Beil. 1,IV,1269

FT-IR 1 (2), 1132:B / Structure Index 1, 478:E:2

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