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259225 Sigma-Aldrich

1,5-Diphenylcarbazide

ACS reagent

Synonym: 1,5-Diphenylcarbohydrazide, sym.-Diphenylcarbazide

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Properties

Related Categories Building Blocks, Carbonyl Compounds, Chemical Synthesis, Hydrazides, Organic Building Blocks More...
grade   ACS reagent
ign. residue   ≤0.05%
mp   170-175 °C(lit.)
  173-176 °C
solubility   aqueous acetone: passes test
suitability   passes test for sensitivity to chromate

Description

Packaging

25, 100 g in glass bottle

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1,5-<WBR>Diphenylcarbazide

Reag. Ph. Eur., ≥98.0%, for metal titration

1,5-<WBR>Diphenylcarbazide

reagent grade

Diphenylcarbazone

for spectrophotometric det. of Cr, Hg, mixture with diphenylcarbazide, ~60%

Dithizone
194832Dithizone

ACS reagent, ≥85.0%

Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
Personal Protective Equipment 
WGK Germany 
3
RTECS 
FF2750000

Protocols & Articles

Peer-Reviewed Papers

References

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Adsorption mechanism of hexavalent chromium by redox within condensed-tannin gel. Nakano Y, Takeshita K, and Tsutsumi T Water Res. 35(2), 496-500, (2001)

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[Investigation of concentration levels of chromium(VI) in bottled mineral and spring waters by high performance ion chromatography technique with application of postcolumn reaction with 1,5-diphenylcarbazide and VIS detection]. Swiecicka D and Garboś S Rocz. Panstw. Zakl. Hig. 59(4), 397-405, (2008)

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Application of multiwalled carbon nanotubes modified by diphenylcarbazide for selective solid phase extraction of ultra traces Cd(II) in water samples and food products. Behbahani M, Bagheri A, Amini MM, et al. Food Chem. 141(1), 48-53, (2013)

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Solid phase extraction of chromium(VI) from aqueous solutions by adsorption of its diphenylcarbazide complex on an Amberlite XAD-4 resin column. Rajesh N, Jalan RK, and Hotwany P J. Hazard. Mater. 150(3), 723-7, (2008)

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Ultra-trace recognition and removal of toxic chromium (VI) ions from water using visual mesocaptor. Shenashen MA, Shahat A, and El-Safty SA J. Hazard. Mater. 244-245, 726-35, (2013)

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Simultaneous separation and determination of trace amounts of Cd(II) and Cu(II) in environmental samples using novel diphenylcarbazide modified nanoporous silica. Bagheri A, Behbahani M, Amini MM, et al. Talanta 89, 455-61, (2012)

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On-line preconcentration and determination of chromium(VI) in waters by high-performance liquid chromatography using precolumn complexation with 1,5-diphenylcarbazide. Padarauskas A, Judzentiene A, Naujalis E, et al. J. Chromatogr. A 808(1-2), 193-9, (1998)

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Photochemical reactions of photosystem II in ethylene glycol. Hillier W, Lukins P, Seibert M, et al. Biochemistry 36(1), 76-85, (1997)

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Continuous automated measurement of hexavalent chromium in airborne particulate matter. Samanta G, Boring CB, and Dasgupta PK Anal. Chem. 73(9), 2034-40, (2001)

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Glycinebetaine protects the D1/D2/Cytb559 complex of photosystem II against photo-induced and heat-induced inactivation. Allakhverdiev SI, Hayashi H, Nishiyama Y, et al. J. Plant Physiol. 160(1), 41-9, (2003)

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Evidence for PSII donor-side damage and photoinhibition induced by cadmium treatment on rice (Oryza sativa L.). Pagliano C, Raviolo M, Dalla Vecchia F, et al. J. Photochem. Photobiol. B, Biol. 84(1), 70-8, (2006)

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Use of a novel histidyl modifier to probe for residues on Tris-treated photosystem II membrane fragments that may bind functional manganese. Ghirardi ML, Preston C, and Seibert M Biochemistry 37(39), 13567-74, (1998)

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Spectroscopic analyses on ROS generation catalyzed by TiO2, CeO2/TiO2 and Fe2O3/TiO2 under ultrasonic and visible-light irradiation. Zou M, Kong Y, Wang J, et al. Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 101, 82-90, (2013)

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Solid phase extraction of chromium(VI) from aqueous solutions by adsorption of its diphenylcarbazide complex on a mixed bed adsorbent (acid activated montmorillonite-silica gel) column. Rajesh N, Mishra BG, and Pareek PK Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 69(2), 612-8, (2008)

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Interactions between diphenylcarbazide, zinc, cobalt, and manganese on the oxidizing side of photosystem II. Ghirardi ML, Lutton TW, and Seibert M Biochemistry 35(6), 1820-8, (1996)

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Dual fluorescence of diphenyl carbazide and benzanilide: effect of solvents and pH on electronic spectra. Sivakumar K, Stalin T, and Rajendiran N Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 62(4-5), 991-9, (2005)

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Determination of total chromium in phosphate rocks by ion chromatography. al-Shawi AW and Dahl R J. Chromatogr. A 850(1-2), 137-41, (1999)

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Effects of carboxyl amino acid modification on the properties of the high-affinity, manganese-binding site in photosystem II. Ghirardi ML, Lutton TW, and Seibert M Biochemistry 37(39), 13559-66, (1998)

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High-specific binding of Fe(II) at the Mn-binding site in Mn-depleted PSII membranes from spinach. Semin BK, Ivanov II, Rubin AB, et al. FEBS Lett. 375(3), 223-6, (1995)

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Kinetic and thermodynamic study of the behaviour of diphenylcarbazide in aqueous solution with pH. Salinas-Hernández P, Rojas-Hernández A, and Ramírez-Silva MT Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 59(11), 2667-75, (2003)

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IR spectroscopic analysis of polymorphism in C13H14N4O. El-Kabbany F, Taha S, and Hafez M Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 78(3), 981-8, (2011)

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Chromium(III) determination with 1,5-diphenylcarbazide based on the oxidative effect of chlorine radicals generated from CCl4 sonolysis in aqueous solution. Borges Sda S, Korn M, and Lima JL Anal. Sci. 18(12), 1361-6, (2002)

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Cr(VI) and Cr(VI)-diphenylcarbazide removal from aqueous solutions using an iron rotating disc electrode. Campos E, Barrera-Díaz C, Ureña-Núñez F, et al. Environ. Technol. 28(1), 1-9, (2007)

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Comparative study of effects of artificial electron donors on the AT-band of photosystem II thermoluminescence. Kultisheva MY, Lovyagina ER, Kuznetsov AM, et al. Biochemistry. (Mosc.) 66(7), 715-20, (2001)

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Electron transfer between exogenous electron donors and reaction center of photosystem 2. Mamedov MD, Kurashov VN, Petrova IO, et al. Biochemistry. (Mosc.) 75(5), 579-84, (2010)

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[Study on the reaction mechanism of the system of Tl(III)-Cu(II)-EDTA-H2O2-DPC]. Sun DM Guang Pu Xue Yu Guang Pu Fen Xi 23(1), 196-8, (2003)

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Merck 14,3321

Beil. 15,IV,182

Aldrich MSDS 1, 823:D / Corp MSDS 1 (1), 1454:C / FT-IR 1 (2), 387:B / FT-IR 2 (2), 3029:B / FT-NMR 1 (2), 1419:B / IR-Spectra (2), 950:C / IR-Spectra (3), 1088:E / NMR-Reference 2 (2), 367:D / RegBook 1 (2), 2043:M / Sigma FT-IR 1 (2), 523:D / Structure Index 1, 325:E:2

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