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410241 Sigma-Aldrich

Sodium perchlorate

ACS reagent, ≥98.0%

Synonym: Hyperchloric acid sodium salt

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Properties

Related Categories Chemical Synthesis, Essential Chemicals, Oxidizing Agents, Perchlorates, Research Essentials,
grade   ACS reagent
assay   ≥98.0%
impurities   ≤0.005% insolubles
pH   6.0-8.0 (25 °C, 5%)
mp   468 °C(lit.)
solubility   water: soluble2.09 g/L at 20 °C
anion traces   chloride (Cl-): ≤0.003%
  sulfate (SO42-): ≤0.002%
cation traces   Ca: ≤0.02%
  Fe: ≤5 ppm
  K: ≤0.05%
  heavy metals (as Pb): ≤5 ppm

Description

Packaging

100, 500 g in glass bottle

2.5 kg in glass bottle

General description

Sodium perchlorate is a water soluble perchlorate salt. It is prepared by electrolyzing aqueous sodium chlorate solution. It is a strong oxidizing agent.1 On impregnating porous silicon with sodium perchlorate it forms an explosive composite which has been investigated.2

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Ultra-high Purity Salts

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Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN 1502 5.1 / PGII
WGK Germany 
1
RTECS 
SC9800000

Documents

Certificate of Analysis

Certificate of Origin

Protocols & Articles

Articles

Determination of Water Content in Sodium perchlorate Using Karl Fischer Titration

Adherent water in salts can be easily determined. It is best to choose a working medium which will prevent the salt from dissolving, e.g. a Methanol-Chloroform mixture with an excess of Chloroform. T...
Keywords: Crystallization, Titrations

Peer-Reviewed Papers

References

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1. Eagleson M. Concise Encyclopedia Chemistry, (1994), 1000

2. Thermal analysis of the exothermic reaction between galvanic porous silicon and sodium perchlorate. Becker CR, et al. ACS Appl. Mater. Interfaces 2(11), 2998-3003, (2010)

Rapid simultaneous determination of telmisartan, amlodipine besylate and hydrochlorothiazide in a combined poly pill dosage form by stability-indicating ultra performance liquid chromatography. Nalwade S, Ranga Reddy V, Durga Rao D, et al. Sci. Pharm. 79(1), 69-84, (2011)

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Scanning electrochemical microscopy: surface interrogation of adsorbed hydrogen and the open circuit catalytic decomposition of formic acid at platinum. Rodri´guez-Lo´pez J and Bard AJ. J. Am. Chem. Soc. 132(14), 5121-5129, (2010)

Synthesis of sulfones using sodium perchlorate as a catalyst under neutral conditions. Bandgar BP, et al. New J. Chem. 26(9), 1105-1107, (2002)

Sodium perchlorate effects on the helical stability of a mainly alanine peptide. Asciutto EK, General IJ, Xiong K, et al. Biophys. J. 98(2), 186-96, (2010)

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Inhibition of the ??-carbonic anhydrase from Streptococcus pneumoniae by inorganic anions and small molecules: Toward innovative drug design of antiinfectives? Peter Burghout et al Bioorg. Med. Chem. 19, 243-8, (2011)

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Ultrafast dynamics of hydrogen bond exchange in aqueous ionic solutions. Park S, Odelius M, and Gaffney KJ J. Phys. Chem. B 113(22), 7825-35, (2009)

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Oxoammonium salt/NaClO2: an expedient, catalytic system for one-pot oxidation of primary alcohols to carboxylic acids with broad substrate applicability. Shibuya M, Sato T, Tomizawa M, et al. Chem. Commun. (Camb.) (13), 1739-41, (2009)

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[Heterotopic transplantation of non-immunogenic trachea populated with recipient bone marrow stromal cells]. Kisilevskiĭ MV, Anisimova NIu, Lebedinskaia OV, et al. Morfologiia. 141(1), 66-70, (2012)

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Fast and continuous preparation of high polymerization degree cellulose nanofibrils and their three-dimensional macroporous scaffold fabrication. Song J, Tang A, Liu T, et al. Nanoscale 5(6), 2482-90, (2013)

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Inhibition studies with anions and small molecules of two novel α-carbonic anhydrases from the bacterial pathogen Salmonella enterica serovar Typhimurium. Daniela Vullo et al Bioorg. Med. Chem. Lett. 21, 3591-5, (2011)

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New insights about the posttranscriptional mechanisms triggered by iodide excess on sodium/iodide symporter (NIS) expression in PCCl3 cells. Serrano-Nascimento C, Calil-Silveira J, Goulart-Silva F, et al. Mol. Cell. Endocrinol. 349(2), 154-61, (2012)

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Significance of oral administration of sodium perchlorate in planning liver-directed radioembolization. Sabet A, Ahmadzadehfar H, Muckle M, et al. J. Nucl. Med. 52(7), 1063-7, (2011)

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Interconnection of salt-induced hydrophobic compaction and secondary structure formation depends on solution conditions: revisiting early events of protein folding at single molecule resolution. Haldar S and Chattopadhyay K J. Biol. Chem. 287(14), 11546-55, (2012)

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Non-specific binding and general cross-reactivity of Y receptor agonists are correlated and should importantly depend on their acidic sectors. Parker MS, Sah R, et al. Peptides 32, 258-265, (2011)

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Effects of Hofmeister ions on the α-helical structure of proteins. Crevenna AH, Naredi-Rainer N, Lamb DC, et al. Biophys. J. 102(4), 907-15, (2012)

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Orientational relaxation dynamics in aqueous ionic solution: polarization-selective two-dimensional infrared study of angular jump-exchange dynamics in aqueous 6M NaClO4. Ji M and Gaffney KJ J. Chem. Phys. 134(4), 044516, (2011)

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Phase system selection with fractional factorial design for purification of recombinant cyanovirin-N from a hydroponic culture medium using centrifugal partition chromatography. Grudzień Ł, Madeira L, Fisher D, et al. J. Chromatogr. A 1285, 57-68, (2013)

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IGF-1 receptor deficiency in thyrocytes impairs thyroid hormone secretion and completely inhibits TSH-stimulated goiter. Ock S, Ahn J, Lee SH, et al. FASEB J. 27(12), 4899-908, (2013)

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Facing the nuclear threat: thyroid blocking revisited. Hänscheid H, Reiners C, Goulko G, et al. J. Clin. Endocrinol. Metab. 96(11), 3511-6, (2011)

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Purification and inhibition studies with anions and sulfonamides of an α-carbonic anhydrase from the Antarctic seal Leptonychotes weddellii. Alessandra Cincinelli et al Bioorg. Med. Chem. 19, 1847-51, (2011)

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Effect of sodium and acetate ions on 8-hydroxyguanine formation in irradiated aqueous solutions of DNA and 2'-deoxyguanosine 5'-monophosphate. Grygoryev D, Moskalenko O, and Zimbrick JD Int. J. Radiat. Biol. 87(9), 974-83, (2011)

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Arsenic speciation in natural and contaminated waters using CZE with in situ derivatization by molybdate and direct UV-detection. Koshcheeva OS, Shuvaeva OV, and Kuznetzova LI Electrophoresis 30(6), 1088-93, (2009)

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Comparative effects of in ovo exposure to sodium perchlorate on development, growth, metabolism, and thyroid function in the common snapping turtle (Chelydra serpentina) and red-eared slider (Trachemys scripta elegans). Eisenreich KM, Dean KM, Ottinger MA, et al. Comp. Biochem. Physiol. C. Toxicol. Pharmacol. 156(3-4), 166-70, (2012)

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Detection of paeoniflorin and albiflorin by immunostaining technique using anti-paeoniflorin monoclonal antibody. Morinaga O, Lu Z, Lin L, et al. Phytochem. Anal. 24(2), 124-8, (2013)

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Study of charge distribution on the surface of biocolloids. Dziubakiewicz E, Hrynkiewicz K, Walczyk M, et al. Colloids Surf. B Biointerfaces 104, 122-7, (2013)

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Notable effects of the metal salts on the formation and decay reactions of α-tocopheroxyl radical in acetonitrile solution. The complex formation between α-tocopheroxyl and metal cations. Kohno Y, Fujii M, Matsuoka C, et al. J. Phys. Chem. B 115(32), 9880-8, (2011)

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Anion inhibition studies of an α-carbonic anhydrase from the living fossil Astrosclera willeyana. Anna Ohradanova et al Bioorg. Med. Chem. Lett. 22, 1314-6, (2012)

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Pseudohypocalcemia caused by perchlorate (Irenat). Durner J, Winkler-Budenhofer U, Gahr S, et al. Clin. Chem. Lab Med. 49(4), 665-7, (2011)

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Electrochemical characterization of riboflavin-enhanced reduction of trinitrotoluene. Sumner JJ and Chu K Sensors (Basel.) 11(11), 10840-50, (2011)

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Impact of ion binding on poly-L-lysine (un)folding energy landscape and kinetics. Xiong K and Asher SA J. Phys. Chem. B 116(24), 7102-12, (2012)

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Effects of water temperature on perchlorate toxicity to the thyroid and reproductive system of Oryzias latipes. Lee S, Ji K, and Choi K Ecotoxicol. Environ. Saf. 108, 311-7, (2014)

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Vibrational spectroscopy and ionic conductivity of polyethylene oxide-NaClO4-CuO nanocomposite. Dey A, Das K, Karan S, et al. Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 83(1), 384-91, (2011)

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The effect of perchlorate medication on point-of-care testing. Hopf S, Bäumel M, Gruber M, et al. Clin. Lab. 58(9-10), 1067-70, (2012)

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Optimization of a method for preparation and repopulation of the tracheal matrix for allogenic transplantation. Kiselevsky MV, Anisimova NY, Lebedinskaya OV, et al. Bull. Exp. Biol. Med. 151(1), 107-13, (2011)

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Merck 14,8653

Aldrich MSDS 1, 1613:B / Corp MSDS 1 (2), 3150:A / FT-IR 2 (3), 4761:D / FT-IR 1 (2), 1253:C / RegBook 1 (3), 3455:G / Sax 6, 2145

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