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92337 Sigma-Aldrich

Bromotrimethylsilane

purum, ≥97.0% (AT)

Synonym: TMBS, Trimethylbromosilane, Trimethylsilyl bromide

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Properties

Related Categories Analytical Reagents, Analytical/Chromatography, Chemical Synthesis, Derivatization Reagents, Derivatization Reagents GC,
InChI Key   IYYIVELXUANFED-UHFFFAOYSA-N
grade   purum
assay   ≥97.0% (AT)
contains   silver wool as stabilizer
refractive index   n20/D 1.424(lit.)
  n20/D 1.424
bp   79 °C(lit.)
density   1.16 g/mL at 25 °C(lit.)
storage temp.   2-8°C

Description

Other Notes

Powerful silylating agent ; Cleavage of ethers ; Smooth cleavage of phosphonic and phosphoric alkyl esters

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Cross-Coupling Guide
Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
Supplemental Hazard Statements 
Reacts violently with water.
RIDADR 
UN 2920 3(8) / PGII
WGK Germany 
3
Flash Point(F) 
77 °F
Flash Point(C) 
25 °C
Protocols & Articles

Articles

Silylating Reagents for GC-MS Compatible Derivatives of NSAIDs

Human and veterinary pharmaceuticals are a group of “emerging” contaminants,1, 2 some of which are produced in increasingly large volumes every year. The amounts produced are reaching quantities simi...
Luis-Alberto Martin
AnalytiX Volume 10 Article 2
Keywords: Anti-inflammatory agents, Derivatizations, Environmental, Gas chromatography, Gas chromatography mass spectrometry, Mass spectrometry, Metabolites, Pesticides, Pharmaceutical, Silylations, Veterinary

Peer-Reviewed Papers
15

References

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