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28471-U Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

  •  eCl@ss 32119290

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Properties

Related Categories β-Glucuronidase Drug Analysis Bundle, Analytical and Industrial Enzymes, Analytical/Chromatography, Biochemicals and Reagents, Capillary GC Columns and Guard Columns/Retention Gaps,
material   fused silica
Beta value   250
df   0.25 μm
application(s)   gas chromatography (GC): suitable
L × I.D.   30 m × 0.25 mm
matrix active group   Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase
column type   capillary non-polar

Description

Frequently Asked Questions

Frequently Asked Questions are available for this Product.

General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
• Bonded and highly crosslinked
• Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
• ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
• ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Legal Information

SLB is a registered trademark of Sigma-Aldrich Co. LLC

Other Notes

Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools

Protocols & Applications

Melamine and Related Compounds in Dog Food Using GC-MS

Price and Availability


Biomedical Applications
Safety & Documentation

Safety Information

Safety Information for this product is unavailable at this time.

Documents

Certificate of Analysis

Protocols & Articles

Articles

Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents Essential Oil on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification, Size-exclusion chromatography

Analysis of Pesticide Residues in Cannabis Using QuEChERS Extraction and Cleanup Followed by GC/MS/MS Analysis

Cannabis (marijuana) has been legalized for recreational and/or medical use by 23 states, the District of Columbia, and the territory of Guam. Thus, regulations regarding its production have become a...
Kathy Stenerson, and Michael Halpenny
Reporter US Volume 34.1
Keywords: Capillary electrophoresis, Fungicides, Gas chromatography, Insecticides, Mass spectrometry, Pesticides, Sample preparations

Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS After Cleanup with a Novel Dual-Layer SPE Cartridge

Turmeric is a plant indigenous to south Asia, with a majority of its production coming from India. The rhizome of the plant is used to produce powdered turmeric, which is used in foods, cosmetics, an...
Katherine K Stenerson, Principal R&D Scientist
Reporter US Volume 34.3
Keywords: Anti-inflammatory agents, Antimicrobials, Capillary electrophoresis, Cosmetics, Gas chromatography, High performance liquid chromatography, Mass selective detector, Mass spectrometry, Pesticides, Reductions, Solid phase extractions

Chemical Standards and Capillary Columns for US EPA Methods 608.1 and 608.2

US EPA Methods 608.1 and 608.2 are extensions of Method 608, and describe the extraction and analysis of certain organochlorine pesticides in municipal and industrial wastewater. This method requires...
Katherine Stenerson
Reporter US Volume 26.5
Keywords: Applications, Certificate, Certificate of Analysis, Chromatography, Degradations, Detection methods, Electron capture detector, Gas chromatography, Methods, Pesticides, Separation, Type

DRO, EPH, ETPH, GRO, PRO, PVOC, STARS, TPH, VPH? Help, I’m Trapped in Alphabet Soup!

The analysis of samples resulting from fuel and oil spills is different from the analyses routinely performed by either a petroleum or an environmental testing laboratory.
Katherine K. Stenerson andMichael D. Buchanan
Reporter US Volume 28.4
Keywords: Chromatography, Degradations, Environmental, Evaporation, Gas chromatography, Help, Methods, Phase transitions, Purge and trap, Sample preparations, Type

Dual-Column GC Analysis of Organochlorine Pesticides on SLB-5ms and SLB-35ms

The analysis of low levels of 20 organochlorine pesticides and 2 surrogate compounds by gas chromatography-electron capture detector (GC-ECD) is routinely performed by analysts in environmental labor...
Lynne Perez-Blanco, Katherine K Stenerson, Michael D Buchanan
Reporter US Volume 33.4
Keywords: Adsorption, Chromatography, Degradations, Detection methods, Electron capture detector, Environmental, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Mass selective detector, Mass spectrometry, Pesticides

EN Method 2005/108/EC: GC Analysis of Pesticide/PAH Compounds on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents EN Method 2005/108/EC: GC Analysis of Pesticide/PAH Compounds on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Pesticides, Purification

Extraction and Analysis of Agricultural Pesticides from Oranges Using the “QuEChERS” Method

The toxicological effects of the chemicals which humans and animals are exposed to daily are of ever-increasing concern. In the last few years, emphasis has been placed on a group of chemicals loosel...
Katherine Stenerson, Robbie Wolford, andOlga Shimelis
Reporter EU Vol 23
Keywords: Agriculture, Catalog, Centrifugation, Food Safety, Fungicides, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Hormones, Insecticides, Mass spectrometry, Methods, Pesticides, Solid phase extractions, Spectra

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Polycyclic Aromatic Hydrocarbons (PAHs) are environmental carcinogenic compounds that can be present in food from many different sources – either naturally or from pollution, packaging, or food prepa...
Olga Shimelis, Katherine Stenerson, Daniel VitkuskeSanja Beyowich1, Brian Boyd1
Reporter US Volume 27.5
Keywords: Environmental, Gas chromatography, Gas chromatography mass spectrometry, High performance liquid chromatography, Mass spectrometry, Solid phase extractions

GC Analysis / Mass Spectrum of Benzo[g,h,i]Perylene (elutes at 325 °C) on SLB®-5ms, from US EPA Method 8270

From our library of Articles, Sigma-Aldrich presents GC Analysis / Mass Spectrum of Benzo[g,h,i]Perylene (elutes at 325 °C) on SLB®-5ms, from US EPA Method 8270
Keywords: Chromatography, Gas chromatography, Purification

GC Analysis of 'Positive List' Chemicals (Mix 1) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 1) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of 'Positive List' Chemicals (Mix 2) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 2) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of 'Positive List' Chemicals (Mix 3) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 3) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of 'Positive List' Chemicals (Mix 4) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 4) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of 'Positive List' Chemicals (Mix 5) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 5) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of 'Positive List' Chemicals (Mix 6) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of 'Positive List' Chemicals (Mix 6) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Pesticides, Purification

GC Analysis of Agricultural Pesticides (Standard) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Agricultural Pesticides (Standard) on SLB®-5ms
Keywords: Agriculture, Chromatography, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Mass spectrometry, Pesticides

GC Analysis of Agricultural Pesticides on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Agricultural Pesticides on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Herbicides, Metabolites, Pesticides, Purification, Size-exclusion chromatography

GC Analysis of Agriculture Pesticides in Orange (Spiked) on SLB®-5ms after QuEChERS Cleanup using Primary-Secondary Amine (PSA)

From our library of Articles, Sigma-Aldrich presents GC Analysis of Agriculture Pesticides in Orange (Spiked) on SLB®-5ms after QuEChERS Cleanup using Primary-Secondary Amine (PSA)
Keywords: Chromatography, Gas chromatography, Pesticides, Purification, Sample preparations, Solid phase extractions

GC Analysis of Bitter Orange Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Bitter Orange Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification

GC Analysis of Bleed Profiles of GC Septa on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Bleed Profiles of GC Septa on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (30 m x 0.25 mm I.D., 0.25 μm)

From our library of Articles, Sigma-Aldrich presents GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (30 m x 0.25 mm I.D., 0.25 μm)
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Cold Pressed Bergamot Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Cold Pressed Bergamot Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Cold Pressed Lemon Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Cold Pressed Lemon Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Cold-Pressed Mandarin Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Cold-Pressed Mandarin Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification

GC Analysis of Distilled Lime Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Distilled Lime Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Durability Test of Molded Thermogreen® LB-2 Septum on SLB-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Durability Test of Molded Thermogreen® LB-2 Septum on SLB-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Estrogenic Compounds on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Estrogenic Compounds on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

GC Analysis of Kennewick Peppermint Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Kennewick Peppermint Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of LSD (TMS Derivatives) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of LSD (TMS Derivatives) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

GC Analysis of Lavender Flower Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Lavender Flower Essential Oil on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Mass selective detector

GC Analysis of Lavender Spike Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Lavender Spike Essential Oil on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Mass selective detector

GC Analysis of Leptosperµm scoparium Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Leptosperµm scoparium Essential Oil on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Native Spearmint Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Native Spearmint Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Neroli Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Neroli Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, High performance liquid chromatography, Mass spectrometry, Purification, Reversed-phase chromatography, Size-exclusion chromatography

GC Analysis of Nitrogen-Containing Herbicides in Water on a 5% Phenyl Column after SPME using 85 μm Polyacrylate Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Nitrogen-Containing Herbicides in Water on a 5% Phenyl Column after SPME using 85 μm Polyacrylate Fiber
Keywords: Chromatography, Gas chromatography, Mass spectrometry, Purification, Size-exclusion chromatography, Solid phase microextractions

GC Analysis of Organophosphorus Pesticides (OP-Pest) in Cabbage, Onion, and Mushrooms on SLB-5ms after SPE using Supelclean™ ENVI-Carb™ II/PSA

From our library of Articles, Sigma-Aldrich presents GC Analysis of Organophosphorus Pesticides (OP-Pest) in Cabbage, Onion, and Mushrooms on SLB-5ms after SPE using Supelclean™ ENVI-Carb™ II/PSA
Keywords: Agriculture, Centrifugation, Chromatography, Degradations, Environmental, Gas chromatography, Nitrogen phosphorus detector, Pesticides, Purification, Sample preparations, Separation, Solid phase extractions

GC Analysis of Organophosphorus Pesticides (OP-Pest) on a 5% Phenyl Column after SPME using 100 μm PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Organophosphorus Pesticides (OP-Pest) on a 5% Phenyl Column after SPME using 100 μm PDMS Fiber
Keywords: Chromatography, Environmental, Gas chromatography, Mass spectrometry, Purification, Solid phase microextractions

GC Analysis of PBDE Flame-Retardant Compounds

Supelco SLB-5ms low-bleed capillary columns and PBDE analytical standards combine for efficient, reliable analysis of these compounds that are of increasing environmental concern.
Roberto FerrariKatherine Stenerson andRainer Walz Ph.D.
Reporter EU Volume 21
Keywords: Automotive, Chromatography, Degradations, Electron capture detector, Electronics, Environmental, Gas chromatography, Gas chromatography mass spectrometry, Hormones, Mass spectrometry, Pesticides, Polymer science, Separation, Solvents

GC Analysis of PCBs in Transformer Oil on a 5%Phenyl Column after SPE using Supelclean™ Sulfoxide

From our library of Articles, Sigma-Aldrich presents GC Analysis of PCBs in Transformer Oil on a 5%Phenyl Column after SPE using Supelclean™ Sulfoxide
Keywords: Chromatography, Gas chromatography, Purification, Sample preparations, Solid phase extractions

GC Analysis of Patchouli Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Patchouli Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Peppermint Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Peppermint Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification

GC Analysis of Pesticide Residues in Cannabis on SLB®-5ms after QuEChERS Extraction then QuEChERS Cleanup using Supel™ QuE Verde

From our library of Articles, Sigma-Aldrich presents GC Analysis of Pesticide Residues in Cannabis on SLB®-5ms after QuEChERS Extraction then QuEChERS Cleanup using Supel™ QuE Verde
Keywords: Adsorption, Chromatography, Gas chromatography, Mass spectrometry, Pesticides, Sample preparations, Solid phase extractions

GC Analysis of Pesticide Residues in Hops on SLB®-5ms after QuEChERS Extraction then QuEChERS Cleanup using Supel™ QuE Verde

From our library of Articles, Sigma-Aldrich presents GC Analysis of Pesticide Residues in Hops on SLB®-5ms after QuEChERS Extraction then QuEChERS Cleanup using Supel™ QuE Verde
Keywords: Adsorption, Chromatography, Gas chromatography, High performance liquid chromatography, Mass spectrometry, Pesticides, Sample preparations, Solid phase extractions

GC Analysis of Pesticides in Spaghetti Sauce on SLB®-5ms after QuEChERS Extraction then Cleanup using Supel QuE PSA/C18

From our library of Articles, Sigma-Aldrich presents GC Analysis of Pesticides in Spaghetti Sauce on SLB®-5ms after QuEChERS Extraction then Cleanup using Supel QuE PSA/C18
Keywords: Chromatography, Gas chromatography, Mass spectrometry, Pesticides, Sample preparations, Solid phase extractions

GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber
Keywords: Chromatography, Gas chromatography, Metabolites, Pesticides, Purification, Solid phase microextractions

GC Analysis of Petitgrain Essential Oil on SLB®-5ms, 50 °C Initial Oven Temp.

From our library of Articles, Sigma-Aldrich presents GC Analysis of Petitgrain Essential Oil on SLB®-5ms, 50 °C Initial Oven Temp.
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Petitgrain Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Petitgrain Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Phenols in Water on a 5% Phenyl Column after SPME using 85 μm Polyacrylate Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Phenols in Water on a 5% Phenyl Column after SPME using 85 μm Polyacrylate Fiber
Keywords: Chromatography, Gas chromatography, Mass spectrometry, Purification, Size-exclusion chromatography, Solid phase microextractions

GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) in Water on a 5% Phenyl Column after SPE using Supelclean™ ENVI-18

From our library of Articles, Sigma-Aldrich presents GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) in Water on a 5% Phenyl Column after SPE using Supelclean™ ENVI-18
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Sample preparations, Solid phase extractions

GC Analysis of Potpourri Fragrance Compounds on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Potpourri Fragrance Compounds on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of QA Test Mix on SLB®-5ms, Three Different Phase Lots

From our library of Articles, Sigma-Aldrich presents GC Analysis of QA Test Mix on SLB®-5ms, Three Different Phase Lots
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Ravensara aromatica Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Ravensara aromatica Essential Oil on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification, Separation, Size-exclusion chromatography

GC Analysis of Resveratrol in Red Wine (Spiked) on SLB®-5ms after SPME using a 85 μm Polyacrylate Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Resveratrol in Red Wine (Spiked) on SLB®-5ms after SPME using a 85 μm Polyacrylate Fiber
Keywords: Chromatography, Derivatizations, Gas chromatography, Mass spectrometry, Purification, Solid phase microextractions

GC Analysis of Resveratrol in Red Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Resveratrol in Red Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber
Keywords: Chromatography, Derivatizations, Gas chromatography, Purification, Solid phase microextractions

GC Analysis of Scotch Spearmint Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Scotch Spearmint Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of Semivolatiles in Drinking Water on a 5% Phenyl Column after SPE using ENVI™-18 DSK

From our library of Articles, Sigma-Aldrich presents GC Analysis of Semivolatiles in Drinking Water on a 5% Phenyl Column after SPE using ENVI™-18 DSK
Keywords: Chromatography, Gas chromatography, Mass spectrometry, Purification, Sample preparations, Solid phase extractions

GC Analysis of Semivolatiles in Water on a 5% Phenyl Column after SPME using 7 μm PDMS

From our library of Articles, Sigma-Aldrich presents GC Analysis of Semivolatiles in Water on a 5% Phenyl Column after SPME using 7 μm PDMS
Keywords: Chromatography, Environmental, Gas chromatography, Mass spectrometry, Purification, Size-exclusion chromatography, Solid phase microextractions

GC Analysis of Sicilian Mandarin Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Sicilian Mandarin Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Separation, Size-exclusion chromatography

GC Analysis of Total Petroleum Hydrocarbons (TPH) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Total Petroleum Hydrocarbons (TPH) on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification

GC Analysis of Trichloroanisole (TCA) and Precursors in Red Wine (Spiked) on SLB-5ms after SPME using 100 μm PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Trichloroanisole (TCA) and Precursors in Red Wine (Spiked) on SLB-5ms after SPME using 100 μm PDMS Fiber
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification, Solid phase microextractions

GC Analysis of Trichloroanisole (TCA) and Precursors in Red Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Trichloroanisole (TCA) and Precursors in Red Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification, Solid phase microextractions

GC Analysis of Trichloroanisole (TCA) and Precursors on SLB®-5ms after SPME using 100 μm a PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Trichloroanisole (TCA) and Precursors on SLB®-5ms after SPME using 100 μm a PDMS Fiber
Keywords: Chromatography, Electron capture detector, Fermentation, Gas chromatography, Mass spectrometry, Purification, Solid phase microextractions

GC Analysis of Trichloroanisole (TCA) in Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Trichloroanisole (TCA) in Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber
Keywords: Chromatography, Gas chromatography, Purification, Solid phase microextractions

GC Analysis of Volatiles in Limoncello on SLB®-5ms after SPME using a 100 μm PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Volatiles in Limoncello on SLB®-5ms after SPME using a 100 μm PDMS Fiber
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Mass spectrometry, Purification, Sample preparations, Solid phase microextractions

GC Analysis of Willamette Peppermint Essential Oil on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Willamette Peppermint Essential Oil on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of a 14-Component Polybrominated Diphenyl Ether (PBDE) Mix on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of a 14-Component Polybrominated Diphenyl Ether (PBDE) Mix on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

GC Analysis of a 17-Component Dioxin Congener Mix on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of a 17-Component Dioxin Congener Mix on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification, Size-exclusion chromatography

GC Analysis of a 17-Component Pesticide Mix on SLB®-5ms (10 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents GC Analysis of a 17-Component Pesticide Mix on SLB®-5ms (10 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis
Keywords: Chromatography, Gas chromatography, Pesticides, Purification

GC Analysis of a 6-Component Tetrachlorodibenzo-p-dioxin (TCDD) Mix on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of a 6-Component Tetrachlorodibenzo-p-dioxin (TCDD) Mix on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification, Size-exclusion chromatography

GC Column Selection Guide

The History of Supelco and the Capillary Column How to Choose a Capillary Column Additional Reading/Product Literature Column Phase Selection by Industry Column Phase Selection by Application Cross-R...
Keywords: Adsorption, Air Monitoring, Chemical industry, Chromatography, Derivatizations, Detection methods, Electron capture detector, Environmental, Gas chromatography, Herbicides, High performance liquid chromatography, Immobilization, Industries, Mass selective detector, Mass spectrometry, Metabolites, Nitrogen phosphorus detector, Pesticides, Pharmaceutical, Purification, Separation, Size-exclusion chromatography, Solid phase extractions, Solid phase microextractions, Solvents, Substitutions

GCxGC Analysis of B20 Biodiesel on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy

From our library of Articles, Sigma-Aldrich presents GCxGC Analysis of B20 Biodiesel on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy
Keywords: Chromatography, Gas chromatography, Size-exclusion chromatography

GCxGC Analysis of C4-C24 FAMEs on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy

From our library of Articles, Sigma-Aldrich presents GCxGC Analysis of C4-C24 FAMEs on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy
Keywords: Chromatography, Gas chromatography, Size-exclusion chromatography

GCxGC Analysis of a 37-Component FAME Mix on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy

From our library of Articles, Sigma-Aldrich presents GCxGC Analysis of a 37-Component FAME Mix on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy
Keywords: Chromatography, Gas chromatography, Size-exclusion chromatography

GCxGC Analysis of a 59-Component Industrial Solvent Mix on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy

From our library of Articles, Sigma-Aldrich presents GCxGC Analysis of a 59-Component Industrial Solvent Mix on SLB®-5ms x SLB-IL60, Non-Polar to Polar Strategy
Keywords: Chromatography, Gas chromatography, Size-exclusion chromatography

Improved Detection & Identification using MSTFA/MSTFA-d9 Derivatization - GC/MS Case Study of Amphetamine

The following was generated with the assistance of an outside source using Sigma-Aldrich products. Technical content was generated and provided by: Dieter Urbach, Bundeskriminalamt (BKA), KT 12 – Zen...
Keywords: Chromatography, Derivatizations, Gas chromatography, Gas chromatography mass spectrometry, Mass spectrometry, Phase transitions, Silylations

Melamine and Related Compounds in Dog Food Using GC-MS

Melamine contamination in food became an issue in recent years after the discovery of it, and related compounds, in pet food and baby formula. It was discovered that melamine was intentionally added ...
Katherine K. Stenerson, Michael D. Buchanan
Reporter US Volume 28.3
Keywords: Centrifugation, Chromatography, Gas chromatography, Gas chromatography mass spectrometry, High performance liquid chromatography, Mass spectrometry, Positron Emission Tomography, Sonication

Molded Thermogreen LB-2 Septa Durability

The injection port septa selected for gas chromatography (GC) use should exhibit low bleed, resist leaks, and be easy to penetrate. Molded Thermogreen LB-2 septa have all these characteristics. Using...
Robert F. Wallace, Gregory A. Baney
Reporter US Volume 28.1
Keywords: Chromatography, Gas chromatography, The Reporter

Resolving by Mass

GC-MS is a powerful tool for the analysis of unknowns and complex mixtures due to the existence of vast GC-MS spectral libraries, making the identification of many compounds possible. In the case of ...
Katherine K. Stenerson
Reporter US Volume 26.5
Keywords: Detection methods, Flame ionization detector, Gas chromatography, Gas chromatography mass spectrometry, MSDS, Mass selective detector, Mass spectrometry, Spectra

Standard Methods 6040D: GC Analysis of Geosmin and 2-MIB on SLB®-5ms after SPME using 50/30 μm DVB/Carboxen/PDMS Fiber

From our library of Articles, Sigma-Aldrich presents Standard Methods 6040D: GC Analysis of Geosmin and 2-MIB on SLB®-5ms after SPME using 50/30 μm DVB/Carboxen/PDMS Fiber
Keywords: Chromatography, Gas chromatography, Purification, Solid phase microextractions

Supelco Low Bleed SLB-5ms Column - New Features and Benefits

In past Reporter articles, we have highlighted the many features and benefi ts of the new SLB-5ms column, especially for US EPA Method 8270. In addition to Method 8270, we have also investigated the ...
Katherine Stenerson, Jay Jones,and Michael D. Buchanan
Reporter EU vol 24
Keywords: Agriculture, Applications, Articles, Chromatography, Clinical, Environmental, Forensic, Fungicides, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Insecticides, Mass spectrometry, Pesticides, Separation, Solid phase microextractions

Testing Food for Fipronil Contamination

In early June, eggs contaminated with the pesticide Fipronil were discovered in Belgium and the Netherlands. A treatment against ticks containing fipronil had been incorrectly used to treat poultry a...
Keywords: Chromatography, Gas chromatography, Gas chromatography mass spectrometry, High performance liquid chromatography, Insecticides, Ion-exchange chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Pesticides, Solvents

The Analysis of Resveratrol in Red Wine by On-Fiber Derivatization/SPME

Resveratrol is a phytoallexin produced by grapes and other plants to increase resistance to fungal infection. Recent research suggests that consumption of resveratrol may reduce the risk of certain c...
Katherine Stenerson
Reporter US Volume 27.4
Keywords: AGE, Chromatography, Derivatizations, Fermentation, Gas chromatography, Gas chromatography mass spectrometry, Mass selective detector, Mass spectrometry, Silylations, Solid phase microextractions

US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on Equity®-1701

From our library of Articles, Sigma-Aldrich presents US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on Equity®-1701
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification

US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SLB®-5ms
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification

US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SPB®-608

From our library of Articles, Sigma-Aldrich presents US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SPB®-608
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm), Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm), Fast GC Analysis
Keywords: Chromatography, Electron capture detector, Gas chromatography, Pesticides, Purification

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms, 340 °C Final Temp.

From our library of Articles, Sigma-Aldrich presents US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms, 340 °C Final Temp.
Keywords: Chromatography, Electron capture detector, Environmental, Gas chromatography, Pesticides, Separation

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms
Keywords: Chromatography, Electron capture detector, Gas chromatography, Pesticides, Purification

US EPA Method 625: GC Analysis of Semivolatiles on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 625: GC Analysis of Semivolatiles on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms
Keywords: Chromatography, Electron capture detector, Gas chromatography, Separation, Size-exclusion chromatography

US EPA Method 8082: GC Analysis of Aroclor 1248 (PCB) on SLB®-5ms and SPB®-608

From our library of Articles, Sigma-Aldrich presents US EPA Method 8082: GC Analysis of Aroclor 1248 (PCB) on SLB®-5ms and SPB®-608
Keywords: Chromatography, Electron capture detector, Gas chromatography, Purification, Size-exclusion chromatography

US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US EPA Method 8141: GC Analysis of Organophosphorus Pesticides (OP-Pest) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 8141: GC Analysis of Organophosphorus Pesticides (OP-Pest) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Nitrogen phosphorus detector, Pesticides, Purification

US EPA Method 8270 (PAH only): GC Analysis of PAHs on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 8270 (PAH only): GC Analysis of PAHs on SLB®-5ms
Keywords: Chromatography, Flame ionization detector, Gas chromatography, Purification

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms, 350 °C Final Oven Temp.

From our library of Articles, Sigma-Aldrich presents US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms, 350 °C Final Oven Temp.
Keywords: Chromatography, Gas chromatography

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms, Comparison to Three Competitive Columns

From our library of Articles, Sigma-Aldrich presents US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms, Comparison to Three Competitive Columns
Keywords: Chromatography, Gas chromatography

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US EPA Method OLM04.2 SVOA: GC Analysis of Semivolatiles on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method OLM04.2 SVOA: GC Analysis of Semivolatiles on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food (Spiked) on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food (Spiked) on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

US FDA LIB 4423: GC Analysis of Melamine and Related Compounds on SLB®-5ms, Method Blank

From our library of Articles, Sigma-Aldrich presents US FDA LIB 4423: GC Analysis of Melamine and Related Compounds on SLB®-5ms, Method Blank
Keywords: Chromatography, Gas chromatography, Purification

US FDA LIB 4423: GC Analysis of Melamine and Related Compounds on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents US FDA LIB 4423: GC Analysis of Melamine and Related Compounds on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

‘Positive List’ Chemicals by GC-MS on the SLB-5ms

In May of 2006, the Japan Ministry of Health, Labour and Welfare (MHLW) introduced regulations for the levels of agricultural chemical residues allowed in plant-based and animal-based foods. This lis...
Katherine K. Stenerson, Takeyoshi Ide, Michael D. Buchanan
Reporter US Volume 27.5
Keywords: Agriculture, Chromatography, Food Safety, Gas chromatography, Gas chromatography mass spectrometry, Help, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Methods, Pesticides, Veterinary

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