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28471-U Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

  •  eCl@ss 32119290

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Properties

Related Categories β-Glucuronidase Drug Analysis Bundle, Analytical and Industrial Enzymes, Analytical/Chromatography, Biochemicals and Reagents, Capillary GC Columns and Guard Columns/Retention Gaps,
material   fused silica
Beta value   250
df   0.25 μm
application(s)   gas chromatography (GC): suitable
L × I.D.   30 m × 0.25 mm
matrix active group   Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase
column type   capillary non-polar

Description

Frequently Asked Questions

Frequently Asked Questions are available for this Product.

General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
• Bonded and highly crosslinked
• Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
• ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
• ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Legal Information

SLB is a registered trademark of Sigma-Aldrich Co. LLC

Other Notes

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Syringes
Vials
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Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools

Protocols & Applications

Melamine and Related Compounds in Dog Food Using GC-MS

Price and Availability


Tools for Small Molecule BioAnalysis
Safety & Documentation

Safety Information

Safety Information for this product is unavailable at this time.

Documents

Certificate of Analysis

Protocols & Articles

Articles

A Selection of New Applications on the Supelco Low Bleed SLB-5ms

In past Reporter articles, we have highlighted the many features and benefi ts of the new SLB-5ms column, especially for US EPA Method 8270. In addition to Method 8270, we have also investigated the ...
Katherine Stenerson, Jay Jones,and Michael D. Buchanan
Reporter EU vol 24
Keywords: Agriculture, Applications, Articles, Chromatography, Clinical, Environmental, Forensic, Fungicides, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Insecticides, Mass spectrometry, Pesticides, Separation, Solid phase microextractions

Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS After Cleanup with a Novel Dual-Layer SPE Cartridge

Turmeric is a plant indigenous to south Asia, with a majority of its production coming from India. The rhizome of the plant is used to produce powdered turmeric, which is used in foods, cosmetics, an...
Katherine K Stenerson
Principal R&D Scientist
Keywords: Anti-inflammatory agents, Antimicrobials, Capillary electrophoresis, Cosmetics, Gas chromatography, High performance liquid chromatography, Mass selective detector, Mass spectrometry, Pesticides, Reductions, Solid phase extractions

Chemical Standards and Capillary Columns for US EPA Methods 608.1 and 608.2

US EPA Methods 608.1 and 608.2 are extensions of Method 608, and describe the extraction and analysis of certain organochlorine pesticides in municipal and industrial wastewater. This method requires...
Katherine Stenerson
Reporter US Volume 26.5
Keywords: Applications, Certificate, Certificate of Analysis, Chromatography, Degradations, Detection methods, Electron capture detector, Gas chromatography, Methods, Pesticides, Separation, Type

DRO, EPH, ETPH, GRO, PRO, PVOC, STARS, TPH, VPH? Help, I’m Trapped in Alphabet Soup!

The analysis of samples resulting from fuel and oil spills is different from the analyses routinely performed by either a petroleum or an environmental testing laboratory.
Katherine K. Stenerson andMichael D. Buchanan
Reporter US Volume 28.4
Keywords: Chromatography, Degradations, Environmental, Evaporation, Gas chromatography, Help, Methods, Phase transitions, Purge and trap, Sample preparations, Type

Dual-Column GC Analysis of Organochlorine Pesticides on SLB-5ms and SLB-35ms

The analysis of low levels of 20 organochlorine pesticides and 2 surrogate compounds by gas chromatography-electron capture detector (GC-ECD) is routinely performed by analysts in environmental labor...
Lynne Perez-Blanco, Katherine K Stenerson, Michael D Buchanan
Reporter US Volume 33.4
Keywords: Adsorption, Chromatography, Degradations, Detection methods, Electron capture detector, Environmental, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Mass selective detector, Mass spectrometry, Pesticides

Extraction and Analysis of Agricultural Pesticides from Oranges Using the “QuEChERS” Method

The toxicological effects of the chemicals which humans and animals are exposed to daily are of ever-increasing concern. In the last few years, emphasis has been placed on a group of chemicals loosel...
Katherine Stenerson, Robbie Wolford, andOlga Shimelis
Reporter EU Vol 23
Keywords: Agriculture, Catalog, Centrifugation, Food Safety, Fungicides, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Hormones, Insecticides, Mass spectrometry, Methods, Pesticides, Solid phase extractions, Spectra

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Polycyclic Aromatic Hydrocarbons (PAHs) are environmental carcinogenic compounds that can be present in food from many different sources – either naturally or from pollution, packaging, or food prepa...
Olga Shimelis, Katherine Stenerson, Daniel VitkuskeSanja Beyowich1, Brian Boyd1
Reporter US Volume 27.5
Keywords: Environmental, Gas chromatography, Gas chromatography mass spectrometry, High performance liquid chromatography, Mass spectrometry, Solid phase extractions

GC Analysis of PBDE Flame-Retardant Compounds

Supelco SLB-5ms low-bleed capillary columns and PBDE analytical standards combine for efficient, reliable analysis of these compounds that are of increasing environmental concern.
Roberto FerrariKatherine Stenerson andRainer Walz Ph.D.
Reporter EU Volume 21
Keywords: Automotive, Chromatography, Degradations, Electron capture detector, Electronics, Environmental, Gas chromatography, Gas chromatography mass spectrometry, Hormones, Mass spectrometry, Pesticides, Polymer science, Separation, Solvents

GC Column Selection Guide

The History of Supelco and the Capillary Column How to Choose a Capillary Column Additional Reading/Product Literature Column Phase Selection by Industry Column Phase Selection by Application Cross-R...
Keywords: Adsorption, Air Monitoring, Chemical industry, Chromatography, Derivatizations, Detection methods, Electron capture detector, Environmental, Gas chromatography, Herbicides, High performance liquid chromatography, Immobilization, Industries, Mass selective detector, Mass spectrometry, Metabolites, Nitrogen phosphorus detector, Pesticides, Pharmaceutical, Purification, Separation, Size-exclusion chromatography, Solid phase extractions, Solid phase microextractions, Solvents, Substitutions

Improved Detection & Identification using MSTFA/MSTFA-d9 Derivatization - GC/MS Case Study of Amphetamine

The following was generated with the assistance of an outside source using Sigma-Aldrich products. Technical content was generated and provided by: Dieter Urbach, Bundeskriminalamt (BKA), KT 12 – Zen...
Keywords: Chromatography, Derivatizations, Gas chromatography, Gas chromatography mass spectrometry, Mass spectrometry, Phase transitions, Silylations

Melamine and Related Compounds in Dog Food Using GC-MS

Melamine contamination in food became an issue in recent years after the discovery of it, and related compounds, in pet food and baby formula. It was discovered that melamine was intentionally added ...
Katherine K. Stenerson, Michael D. Buchanan
Reporter US Volume 28.3
Keywords: Centrifugation, Chromatography, Gas chromatography, Gas chromatography mass spectrometry, High performance liquid chromatography, Mass spectrometry, Positron Emission Tomography, Sonication

Molded Thermogreen LB-2 Septa Durability

The injection port septa selected for gas chromatography (GC) use should exhibit low bleed, resist leaks, and be easy to penetrate. Molded Thermogreen LB-2 septa have all these characteristics. Using...
Robert F. Wallace, Gregory A. Baney
Reporter US Volume 28.1
Keywords: Chromatography, Gas chromatography, The Reporter

Resolving by Mass

GC-MS is a powerful tool for the analysis of unknowns and complex mixtures due to the existence of vast GC-MS spectral libraries, making the identification of many compounds possible. In the case of ...
Katherine K. Stenerson
Reporter US Volume 26.5
Keywords: Detection methods, Flame ionization detector, Gas chromatography, Gas chromatography mass spectrometry, MSDS, Mass selective detector, Mass spectrometry, Spectra

The Analysis of Resveratrol in Red Wine by On-Fiber Derivatization/SPME

Resveratrol is a phytoallexin produced by grapes and other plants to increase resistance to fungal infection. Recent research suggests that consumption of resveratrol may reduce the risk of certain c...
Katherine Stenerson
Reporter US Volume 27.4
Keywords: AGE, Chromatography, Derivatizations, Fermentation, Gas chromatography, Gas chromatography mass spectrometry, Mass selective detector, Mass spectrometry, Silylations, Solid phase microextractions

‘Positive List’ Chemicals by GC-MS on the SLB-5ms

In May of 2006, the Japan Ministry of Health, Labour and Welfare (MHLW) introduced regulations for the levels of agricultural chemical residues allowed in plant-based and animal-based foods. This lis...
Katherine K. Stenerson, Takeyoshi Ide, Michael D. Buchanan
Reporter US Volume 27.5
Keywords: Agriculture, Chromatography, Food Safety, Gas chromatography, Gas chromatography mass spectrometry, Help, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Methods, Pesticides, Veterinary

Related Content

How to Choose a Capillary GC Column

An optimized chromatographic separation begins with the column. The selection of the proper capillary column for any application should be based on four significant factors: stationary phase, column ...
How to Choose a Capillary GC Column
Keywords: Chromatography, Condensations, Gas chromatography, Immobilization, Mass spectrometry, Pesticides, Separation, Size-exclusion chromatography, Solid phase microextractions, Solvents, Vaporization

Peer-Reviewed Papers
15

References

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