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57017 Supelco

Supelclean LC-SAX SPE Tube

bed wt. 500 mg, volume 3 mL, pkg of 54 ea

Synonym: SAX tube

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Properties

Related Categories Analytical/Chromatography, Ion-Exchange Supelclean SPE Products, Sample Preparation & Purification, Solid Phase Extraction (SPE), Supelclean ENVI and Supelclean SPE Cartridges,
composition   bed wt., 500 mg
packaging   pkg of 54 ea
volume   3 mL
matrix   silica gel
matrix active group   SAX phase
  quaternary amine, Cl- counterion
diameter   40-45 μm
pore size   60 Å
mode of chromatography   Ion exchange
  Ion exchange

Description

Frequently Asked Questions

Frequently Asked Questions are available for this Product.

Legal Information

Supelclean is a trademark of Sigma-Aldrich Co. LLC

Price and Availability


All labs need water

Non-Sterile Millex Syringe Filters
Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
Personal Protective Equipment 
RIDADR 
NONH for all modes of transport
WGK Germany 
3

Documents

Certificate of Analysis

Frequently Asked Questions

Which document(s) contains shelf-life or expiration date information for a given product?
If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis. These documents are located on the product detail page under Useful Links & Tools. Click on the following link to search for a Certificate of Analysis. Please click the following link to see the details on our Product Dating Information.
How do I get lot-specific information or a Certificate of Analysis?
A Certificate of Analysis is available by lot number and can be obtained through our Advanced Search Option: http://www.sigmaaldrich.com/catalog/AdvancedSearchPage.do
What is the functional group on the Supelclean LC-SAX SPE, Product 57017?
The Supelclean LC-SAX SPE functional group is an aliphatic quaternary amine bonded to silica, with a chloride (Cl-) counter-ion; the capacity is approximately 0.2 meq/g (milliequivalents per gram).
What is the conditioning procedure for the 500mg/3mL Supelclean LC-SAX SPE, Product 57017?
How can analytes be eluted from the Supelclean LC-SAX SPE, Product 57017?
The most common elution strategy with the Supelclean LC-SAX SPE is by pH manipulation.  Start by using a buffer with the pH adjusted to at least 2 pH units above the molecule’s pKa.  Methanol may be added to disrupt secondary interactions. Elute with 100 μL aliquots, at a reduced flow rate of approximately 1-2 drops/second.
How do I find price and availability?
There are several ways to find pricing and availability for our products.  Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers. 
What is the Department of Transportation shipping information for this product?
Transportation information can be found in Section 14 of the product's (M)SDS. To access the shipping information for this material, use the link on the product detail page for the product, or search here. 
My question is not addressed here, how can I contact Technical Service for assistance?
Use the option to the right to "Ask a Question" by email of a Technical Service Scientist.
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Protocols & Articles

Articles

Solid Phase Extraction: Ion Exchange Methodology

In order for electrostatic retention to occur, both analyte and sorbent functional groups must be in their ionized form. This is done through strict pH control of the sample matrix. For basic analyte...
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Solid Phase Extraction: Normal Phase Methodology

In order for polar retention to occur between the sorbent and the sample, the analyte must be introduced to the SPE device in a non-polar sample or mobile phase environment. Therefore, typical sample...
Keywords: Cosmetics, Fractionation, Gas chromatography, Separation, Solid phase extractions, Solvents, Sonication

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Solid Phase Extraction: Fundamentals and Recent Developments [Webinar]

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