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G001357 Supelco

GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap

application for GC

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Related Categories Analytical/Chromatography, Applications, Capillary GC Columns and Guard Columns/Retention Gaps, Capillary GC Columns, by industry / application, Capillary GC Columns, by name,
test parameters   sample/matrix: 50 ppb each component in 5mL of water
  purge trap: VOCARB 3000
  purge: 40 mL/min for 11 min at ambient temperature
  desorption temp.: 210 °C for 2 min
  bake: 260 °C for 10 min
  transfer line/valve temp.: 110 °C
  column: SPB-624, 60 m x 0.32 mm ID, 1.8 μm (24251)
  oven: 35 °C (8 min), 5 °C/min to 100 °C, 15 °C/min to 220 °C (5 min)
  inj. temp.: 230 °C
  scan range: m/z 41-400
  carrier gas: helium, 1.2 mL/min constant
  injection: split ~18:1
  instrument: OI 4560
suitability   application for GC
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