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G003579 Supelco

US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms

application for GC

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Related Categories Analytical/Chromatography, Applications, Beverage Analysis (Water), Capillary GC Columns and Guard Columns/Retention Gaps, Capillary GC Columns, by industry / application,
test parameters   column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
  oven: 45 °C (1 min), 50 °C/min to 130 °C (1 min), 12 °C/min to 180 °C, 7 °C/min to 240 °C, 12 °C/min to 330 °C (2 min)
  inj. temp.: 275 °C
  MSD interface: 330 °C
  scan range: m/z = 45-450
  carrier gas: helium, 0.9 mL/min., constant flow
  injection: 1 μL pulsed splitless (15 psi until 0.20 min) (1.0 min)
  liner: 4 mm I.D., single taper
  sample: 2 ppm, in ethyl acetate, of a 102 component semivolatile standard plus 3 surrogate and 3 internal standard compounds (at 5 ppm)
suitability   application for GC
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