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G004732 Supelco

HPLC Analysis of cis/trans-Dothiepin Enantiomers on Astec® CYCLOBOND® I 2000 AC

application for HPLC

Properties

Related Categories All Pharmaceutical Applications, Analytical/Chromatography, Antidepressants, Applications, Chiral Applications,
test parameters   column: CYCLOBOND I 2000 AC, 25 cm x 4.6 mm I.D., 5 μm particles (20124AST)
  mobile phase: [A] 1.0% triethylamine acetate, pH 4.1; [B] acetonitrile; (85:15, A:B)
  flow rate: 1 mL/min
  column temp.: 22 °C
  detector: UV, 254 nm
  injection: 2 μL
  sample: 1 mg/mL in methanol
peak 1: 9.48 min.
peak 2: 12.48 min.
suitability   application for HPLC
Featured Industry   Pharmaceutical (small molecule)

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Description

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Astec is a registered trademark of Sigma-Aldrich Co. LLC

CYCLOBOND is a registered trademark of Sigma-Aldrich Co. LLC

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