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US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food (Spiked) on SLB®-5ms

application for GC

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Related Categories Adulterants, Amines, Analytical/Chromatography, Applications, Capillary GC Columns and Guard Columns/Retention Gaps,
test parameters   column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
  oven: 115 °C (3 min), 10 °C/min to 325 °C (6 min)
  inj. temp.: 250 °C
  MSD interface: 325 °C
  scan range: SIM
  carrier gas: helium, 1 mL/min., constant
  injection: 1 μLsplitless
  liner: 4 mm I.D. single taper
  sample: TMS derivatives of melamine and related compounds (extract of dog food spiked with each analyte at 10 μg/g, with I.S. added at 1000 ng/mL, in pyridine:sylon BFT)
suitability   application for GC
Featured Industry   Food and Beverages

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