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 Vol. 2, No. 3
Products for NMR
Click here to download PDF version. (914 KB)
Introduction / NMR Solvents / NMR Tubes / Spectral Viewer / Synthesis / Reference Books
NMR Solvents
Deuterated NMR Solvents / High Purity Solvents / Anhydrous NMR solvents
NMR Reference Standards / LC-NMR Reference Standards / LC-NMR solvents
Deuterated NMR Solvents
Aldrich and Isotec have shared manufacturing methods to offer a complete line of products for the NMR industry. We continually look for ways to improve our manufacturing process so we can offer you the best NMR solvent quality possible. Take a look at these NMR solvents that now have higher isotopic enrichment.
| Cat. No. |
Product Information |
Unit Sizes |
| Chloroform-d (previous isotopic purity 99.8 atom % D) |
| 15,182-3 |
Chloroform-d, 99.9 atom % D |
screw-cap |
50g |
| |
|
screw-cap |
100g |
| |
|
screw-cap |
10 x 100g |
| |
|
Sure/Seal™ |
150g |
| |
|
screw-cap |
250g |
| 23,689-6 |
Chloroform-d, 99.9 atom % D |
ampule |
10 x 1.0mL |
| 44,133-3 |
Chloroform-d, 99.9 atom % D |
ampule |
10 x 0.75mL |
| 52,201-5 |
Chloroform-d, 99.9 atom % D |
ampule |
10 x 0.60mL |
| 30,873-0 |
Chloroform-d, 99.9 atom % D |
ampule |
5 x 0.5mL |
| 22,578-9 |
Chloroform-d, 99.9 atom % D (contains 0.03% TMS) |
screw-cap |
100g |
| |
|
screw-cap |
10 x 100g |
| |
|
Sure/Seal™ |
150g |
| |
|
screw-cap |
500g |
| 42,366-1 |
Chloroform-d, 99.9 atom % D (contains 0.03% v/v TMS) |
ampule |
10 x 1.0mL |
| 15,183-1 |
Chloroform-d, 99.9 atom % D (contains 1% v/v TMS) |
screw-cap |
50g |
| |
|
screw-cap |
100g |
| |
|
screw-cap |
10 x 100g |
| |
|
Sure/Seal™ |
150g |
| |
|
screw-cap |
250g |
| TOP |
| Dichloromethane-d2 (previous isotopic purity 99.8 atom % D) |
| 44,432-4 |
Dichloromethane-d2, 99.9 atom % D |
ampule |
5g |
| |
|
ampule |
10g |
| |
|
ampule |
25g |
| 52,211-2 |
Dichloromethane-d2, 99.9 atom % D |
screw-cap |
10g |
| 44,610-6 |
Dichloromethane-d2, 99.9 atom % D |
ampule |
10 x 0.75mL |
| 52,203-1 |
Dichloromethane-d2, 99.9 atom % D |
ampule |
10 x 0.6mL |
| 53,050-6 |
Dichloromethane-d2, 99.9 atom % D (contains 0.1% v/v |
ampule |
1g |
| |
TMS) |
ampule |
5g |
| |
|
ampule |
10g |
| |
|
ampule |
25g |
TOP
NEW High Purity Solvents
Aldrich now offers high purity NMR solvents that have minimum isotopic purity levels of 99.996 atom % D or better. These solvents offer the highest isotopic enrichment available for NMR applications where purity is absolutely crucial.
| Cat. No. |
Product Information |
Unit Sizes |
| EXTRA (minimum 99.996 atom % D) |
| 61,339-8 |
Deuterium oxide, EXTRA |
ampule |
10 x 0.75mL |
| 61,230-8 |
(Methyl sulfoxide)-d6, EXTRA |
ampule |
10 x 0.25mL |
| |
|
ampule |
10 x 0.50mL |
| |
|
ampule |
10 x 0.75mL |
| |
| ULTRA-D (minimum 99.999 atom % D) |
| 61,340-1 |
Deuterium oxide, ULTRA-D |
ampule |
10g |
| 57,023-0 |
Deuterium oxide, ULTRA-D |
ampule |
10 x 0.75mL |
| |
| Improved DMSO-d6 Now Lower water |
| We have taken steps to improve the water levels in all of our DMSO listings. Order some today and experience the difference. We have also recently added DMSO-d6, 99.9 atom % D, “Special HOH”. D2O and HOD levels are kept to a minimum to avoid deuterium exchange with easily exchangeable protons in your sample. |
| 61,232-4 |
(Methyl sulfoxide)-d6, 99.9 atom % D Special |
ampule |
25g |
| |
HOH |
ampule |
10 x 0.75mL |
| |
|
ampule |
50g |
TOP
NEW Anhydrous NMR solvents
Extra peaks arising from water impurities can mask areas of your NMR spectrum, resulting in valuable structural information that may be hidden from view. The area of the NMR spectrum where water usually appears (from 1-5ppm,depending on the solvent), is also a common area for proton signals arising from important functionalities such as alkanes, alkenes, amines, and alcohols. Aldrich now offers anhydrous NMR solvents that can take the guesswork out of structure determination in this range for you. Aldrich produces every anhydrous deuterated solvent to tight water specifications. Each solvent is produced using the most modern techniques available and are continually monitored to ensure that extremely low water specifications are maintained.
| Cat. No. |
Product Information |
Unit Sizes |
Max ppm
of Water |
| Ampule Packs |
| 56,955-0 |
Acetonitrile-d3, 99.8 atom % D, anhydrous |
10 x 1.0mL |
10 |
| |
|
5 x 1.0mL |
|
| 56,956-9 |
Chloroform-d, 99.8 atom % D, anhydrous |
10 x 1.0mL |
10 |
| |
|
5 x 1.0mL |
|
| 56,953-4 |
Methyl-d3 alcohol-d, 99.8+ atom % D, anhydrous |
10 x 1.0mL |
100 |
| |
|
5 x 1.0mL |
|
| 56,958-5 |
(Methyl sulfoxide)-d6, 99.9 atom % D, anhydrous |
10 x 1.0mL |
50 |
| |
|
5 x 1.0mL |
|
| |
| Screw-Cap Bottles |
| 57,070-2 |
Acetonitrile-d3, 99.8 atom % D, anhydrous |
50g |
10 |
| 57,068-0 |
Benzene-d6, 99.6 atom % D, anhydrous |
50g |
10 |
| 57,069-9 |
Chloroform-d, 99.8 atom % D, anhydrous |
50g |
10 |
| 57,072-9 |
Methyl-d3 alcohol-d, 99.8+ atom % D, anhydrous |
50g |
100 |
| 57,067-2 |
(Methyl sulfoxide)-d6, 99.9 atom % D, anhydrous |
50g |
50 |
| 57,071-0 |
Toluene-d8, 99.6 atom % D, anhydrous |
50g |
10 |
TOP
NMR Reference Standards
We offer an extensive list of NMR reference standards in a variety of tube lengths. If there is a special mix you are interested in that we do not offer, please contact our Technical Services department at 800-231-8327(USA), or your local Sigma-Aldrich sales office.
| Cat. No. |
Product Information |
Tube Size |
| 61,177-8 |
1% Chloroform in acetone-d6, 99.9 atom % D |
3mm x 8in |
| 61,303-7 |
1% Chloroform in acetone-d6, 99.9 atom % D |
4mm x 8in |
| 61,177-8 |
1% Chloroform in acetone-d6, 99.9 atom % D |
3mm x 8in |
| 61,303-7 |
1% Chloroform in acetone-d6, 99.9 atom % D |
4mm x 8in |
| 61,174-3 |
1% Chloroform in acetone-d6, 99.9 atom % D |
10mm x 8in |
| 61,330-4 |
2% Chloroform in chloroform-d, 99.9 atom % D |
3mm x 8in |
| 61,331-2 |
2% Chlorform in chloroform-d, 99.9 atom % D |
5mm x 8in |
| 61,178-6 |
5% Chloroform in acetone-d6, 99.9 atom % D |
3mm x 8in |
| 61,183-2 |
5% Chloroform in acetone-d6, 99.9 atom % D |
4mm Nano tube |
| 61,185-9 |
20% Chloroform in acetone-d6, 99.8 atom % D |
5mm x 8in |
| 61,183-2 |
5% Chloroform in acetone-d6, 99.9 atom % D |
4mm Nano tube |
| 61,185-9 |
20% Chloroform in acetone-d6, 99.8 atom % D |
5mm x 8in |
| 61,251-0 |
5% 1,2-Dichlorobenzene in acetone-d6, 99.9 atom % D |
5mm x 8in |
| 61,211-1 |
40% 1,4-Dioxane in benzene-d6, 99.6 atom % D |
3mm x 8in |
| 61,179-4 |
40% 1,4-Dioxane in benzene-d6, 99.6 atom % D |
4mm Nano tube |
| 61,207-3 |
40% 1,4-Dioxane and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D |
3mm x 8in |
| 61,190-5 |
40% 1,4-Dioxane and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D |
5mm x 8in |
| 61,182-4 |
40% 1,4-Dioxane, and 5mg/mL chromium(III) acetylacetonate in benzene-d6, 99.6 atom % D |
4mm Nano tube |
| 61,304-5 |
0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D |
4mm x 8in |
| 61,026-5 |
0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D |
10mm x 8in |
| 61,180-8 |
0.1% Ethylbenzene and 0.01% TMS in chloroform-d, 99.9 atom % D |
4mm Nano tube |
| 61,248-0 |
0.1% Ethylbenzene, 0.01% TMS and 0.1mg/mL chromium(III) acetylacetonate in chloroform-d, 99.9 atom % D |
5mm x 8in |
| 61,293-6 |
5% Ethylbenzene and 2% TMS in chlorform-d, 99.9 atom % D |
5mm x 7in |
| 61,270-7 |
45% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D |
3mm x 8in |
| 61,189-1 |
45% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D |
5mm x 8in |
| 61,333-9 |
90% Formamide in (methyl sulfoxide)-d6, 99.9 atom % D |
3mm x 8in |
| 61,208-1 |
0.1mg/mL Gadolinium(III) chloride, 0.1% DSS and 1% water in deuterium oxide, 99.9 atom % D |
3mm x 8in |
| 61,194-8 |
0.1mg/mL Gadolinium(III) chloride, 0.1% DSS and 1% water in deuterium oxide, 99.9 atom % D |
8mm x 8in |
| 61,181-6 |
0.1mg/mL Gadolinium(III) chloride in deuterium oxide, 99.9 atom % D |
4mm Nano tube |
| 61,192-1 |
25% Hexamethyldisiloxane in benzene-d6, 99.6 atom % D |
5mm x 8in |
| 61,329-0 |
50% Menthol and 0.5% chromium(III) acetylacetonate in chloroform-d, 99.9 atom % D |
5mm x 8in |
| 61,216-2 |
85% Phosphoric acid in deuterium oxide, 99.9 atom % D |
5mm x 8in coaxial tube |
| 61,191-3 |
0.2M Potassium fluoride and 90% water in deuterium oxide, 99.9 atom % D |
10mm x 8in |
| 61,268-5 |
0.05% a,a,a-Trifluorotoluene in benzene-d6, 99.6 atom % D |
3mm x 8in |
| 61,318-5 |
0.05% a,a,a-Trifluorotoluene in benzene-d6, 99.6 atom % D |
4mm x 8in |
| 61,117-9 |
0.0485M Triphenylphosphate in chlorform-d, 99.9 atom % D |
8mm x 8in |
| 61,173-5 |
0.0485M Triphenylphosphate in chloroform-d, 99.9 atom % D |
10mm x 8in |
TOP
LC-NMR Reference Standards
| Cat. No. |
Product Information |
Unit Size |
| 61,244-8 |
1% Chloroform in acetone-d6, 99.9 atom % D |
screw-cap |
50mL |
| 61,302-9 |
50mM Sodium acetate and 1% water in deuterium oxide, 99.9 atom % D |
screw-cap |
50mL |
| 61,242-1 |
1% Water in deuterium oxide, 99.9 atom % D |
screw-cap |
250mL |
TOP
LC-NMR Solvents
| Cat. No. |
Product Information |
Unit Size |
| 53,089-1 |
1% Chloroform in acetone-d6, 99.9 atom % D |
screw-cap |
50mL |
| 61,302-9 |
Acetone-d6, 99.5 atom % D |
GL-45 bottle |
1L |
| 53,088-3 |
Acetonitrile-d3, 99.8 atom % D |
GL-45 bottle |
1L |
| 56,310-2 |
Acetonitrile-d3, 99.8 atom % D (contains 15-20% D2O) |
GL-45 bottle |
1L |
| 53,086-7 |
Deuterium oxide, 99.9 atom % D |
GL-45 bottle |
1L |
| 53,087-5 |
Methyl-d3 alcohol-d, 99.8+ atom % D |
GL-45 bottle |
1L |
| 34955 |
Acetonitrile NMR CHROMASOLV® |
GL-45 bottle |
500mL |
| |
|
|
6 x 500mL |
| |
|
|
1L |
| |
|
|
6 x 1L |
TOP |
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