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 Vol. 2, No. 3
Products for NMR
Click here to download PDF version. (914 KB)
Introduction / NMR Solvents / NMR Tubes / Spectral Viewer / Synthesis / Reference Books
NMR Tubes
Aldrich NMR Tubes / Wilmad NMR Tubes / Wilmad Screw Cap NMR Tubes
Aldrich NMR Tubes
Every Aldrich premium-quality NMR tube is inspected and gauged to meet published specifications.
- Aldrich Statement of Conformance stamped on each box of tubes
- Made of ASTM Type I borosilicate glass* for compatibility with ground joints, valves, and vacuum racks
- Precision ground and highly polished for spinning stability and highest resolution
- Thin-wall glass with round-bottoms
- Sandblasted marking spot for labelling samples
*Except disposable grade NMR tubes.
| NMR TUBE SELECTION GUIDE
Choose the NMR tube grade that most closely matches the frequency (in MHz) of the spectrometer.
| Aldrich Grade |
MHz |
Applications |
Cross Ref. No.
(5mm tubes) |
| Wilmad |
Kontes |
| Disposable |
30 |
Student labs, basic studies |
WG-Economy |
— |
| Series 30 |
30 |
Student labs, basic studies |
505-PS |
897200 |
| Series 200 |
60 to 270 |
Lower field studies |
506-PP |
897205 |
| Series 300 |
60 to 360 |
Routine applications |
507-PP |
897220 |
| Series 400 |
200 to 500 |
High-field, multiple-scan FT-NMR |
528-PP |
897235 |
| Series 500 |
500+ |
Ultra-high resolution |
535-PP |
897240 |
| Series 800 |
600 to 800 |
Highest resolution and performance |
541-PP |
897245 |
|
 |
| Grade |
L (in.) |
Wall uniformity
(in., TIR) |
Camber (in.) |
Cat. No. |
| 3mm Microsample NMR tubes — 0.012in. wall thickness (Pkg=5 tubes) |
| Series 300 |
7 |
0.0020 |
0.0010 |
Z41,290-2 |
| |
8 |
0.0020 |
0.0011 |
Z41,291-0 |
| Series 400 |
7 |
0.0010 |
0.0005 |
Z41,292-9 |
| |
8 |
0.0010 |
0.0006 |
Z41,293-7 |
| Series 500 |
7 |
0.0005 |
0.00025 |
Z41,294-5 |
| |
8 |
0.0005 |
0.00035 |
Z41,295-3 |
| 5mm NMR tubes — 0.015in. wall thickness (Pkg=5 tubes) |
| Disposable |
7 |
— |
— |
Z41,277-5 |
| Series 30 |
7 |
0.0030 |
0.002 |
Z41,278-3 |
| Series 200 |
7 |
0.0025 |
0.002 |
Z41,279-1 |
| Series 300 |
7 |
0.0020 |
0.0010 |
Z41,280-5 |
| Series 200 |
7 |
0.0025 |
0.002 |
Z41,279-1 |
| |
8 |
0.0020 |
0.0011 |
Z41,281-3 |
| |
9 |
0.0020 |
0.0012 |
Z41,282-1 |
| Series 400 |
7 |
0.0010 |
0.0005 |
Z41,284-8 |
| |
8 |
0.0010 |
0.0006 |
Z41,285-6 |
| Series 500 |
7 |
0.0005 |
0.00025 |
Z41,286-4 |
| |
8 |
0.0005 |
0.00035 |
Z41,287-2 |
| Series 800 |
7 |
0.0002 |
0.00015 |
Z41,288-0 |
| |
8 |
0.0002 |
0.00015 |
Z41,289-9 |
| 10mm NMR tubes — 0.018in. wall thickness (Pkg=5 tubes) |
| Series 200 |
7 |
0.0030 |
0.0015 |
Z41,296-1 |
| Series 400 |
7 |
0.0015 |
0.0005 |
Z41,298-8 |
| TIR-Total Indicator Reading |
TOP
Wilmad NMR Tubes
Made of Pyrex borosilicate glass (unless otherwise noted) for compatibility with ground joints, valves, and vacuum racks. Precision ground and highly polished for spinning stability and highest resolution. Tubes have round bottoms and include a sandblasted marking spot for labeling samples. Tubes that are 9in. L are for making standards and for use with tip-off manifolds.
| SELECTION GUIDE
| Grade |
Applications |
| Precision |
Frequently used as disposable tubes by students and in rudimentary studies |
| Imperial |
60 to 270MHz, lower field studies |
| Ultra-Imperial |
60 to 360MHz, for routine applications |
| Royal Imperial |
200 to 500MHz, unsurpassed performance in this range |
| Emperor |
500MHz or higher, offers highest precision available |
|
| 3mm Microsample NMR tubes — 0.012in. wall thickness (Pkg=5 tubes) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 300MHz tubes |
| 7 |
51/25 |
307-PP-7 |
Z27,432-1 |
| 8 |
51/25 |
307-PP-8 |
Z27,434-8 |
| 9 |
51/25 |
307-PP-9 |
Z27,435-6 |
| 360MHz tubes |
| 7 |
25/25 |
327-PP-7 |
Z27,186-1 |
| 8 |
25/25 |
327-PP-8 |
Z27,436-4 |
| 9 |
25/25 |
327-PP-9 |
Z27,437-2 |
| 400MHz tubes |
| 7 |
25/13 |
328-PP-7 |
Z27,438-0 |
| 8 |
25/13 |
328-PP-8 |
Z27,439-9 |
| 9 |
25/13 |
328-PP-9 |
Z27,440-2 |
| 500MHz tubes |
| 7 |
13/6 |
335-PP-7 |
Z27,441-0 |
| 8 |
13/6 |
335-PP-8 |
Z27,442-9 |
| 9 |
13/6 |
335-PP-9 |
Z27,443-7 |
|
TOP
5mm amber NMR tubes — 0.015in. wall thickness (Pkg=1 tube) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 100MHz tube |
| 7 |
76/51 |
505-PS-7 |
Z28,225-1 |
| 360MHz tubes |
| 7 |
51/25 |
507-PP-7 |
Z28,227-8 |
| 7 |
25/25 |
527-PP-7 |
Z28,228-6 |
|
TOP
5mm disposable NMR tubes — 0.015in. wall thickness, N51 glass (Pkg=100 tubes) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 100MHz tubes |
| 7 |
76/76 |
HIP-7 |
Z51,414-4 |
| 8 |
76/76 |
HIP-8 |
Z51,415-2 |
|
TOP
5mm economy NMR tubes — 0.015in. wall thickness. WG series made of N51 glass. (Pkg=5 tubes) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 100MHz tubes |
| 7 |
76/76 |
WG-5-7 |
Z27,627-8 |
| 8 |
76/76 |
WG-5-8 |
Z27,628-6 |
| 9 |
76/76 |
WG-5-9 |
Z27,629-4 |
| 7 |
76/76 |
512-5-7 |
Z27,630-8 |
| 8 |
76/76 |
512-5-8 |
Z27,631-6 |
| 9 |
76/76 |
512-5-9 |
Z27,632-4 |
| 7 |
51/51 |
506-IM-7 |
Z51,412-8 |
| 8 |
51/51 |
506-IM-8 |
Z51,413-6 |
|
TOP
5mm standard NMR tubes — 0.015in. wall thickness (Pkg=5 tubes) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 100MHz tubes |
| 7 |
76/51 |
505-PS-7 |
Z27,198-5 |
| 8 |
76/51 |
505-PS-8 |
Z27,444-5 |
| 9 |
76/51 |
505-PS-9 |
Z27,445-3 |
| 7 |
51/51 |
506-PP-7 |
Z28,602-8 |
| 8 |
51/51 |
506-PP-8 |
Z28,603-6 |
| 9 |
51/51 |
506-PP-9 |
Z28,604-4 |
| 200MHz tube |
| 7 |
76/51 |
503-PS-7** |
Z41,035-7 |
| 360MHz tubes |
| 7 |
51/25 |
507-PP-7 |
Z27,199-3 |
| 8 |
51/25 |
507-PP-8 |
Z27,446-1 |
| 9 |
51/25 |
507-PP-9 |
Z27,211-6 |
| 7 |
51/13 |
526-PP-7 |
Z27,448-8 |
| 8 |
51/13 |
526-PP-8 |
Z27,449-6 |
| 9 |
51/13 |
526-PP-9 |
Z27,451-8 |
| 7 |
25/25 |
527-PP-7 |
Z27,427-5 |
| 8 |
25/25 |
527-PP-8 |
Z27,452-6 |
| 9 |
25/25 |
527-PP-9 |
Z27,453-4 |
| 400MHz tubes |
| 7 |
25/13 |
528-PP-7 |
Z27,201-9 |
| 8 |
25/13 |
528-PP-8 |
Z27,429-1 |
| 9 |
25/13 |
528-PP-9 |
Z27,454-2 |
| 500 MHz tubes |
| 7 |
13/6 |
535-PP-7 |
Z27,202-7 |
| 7 |
13/6 |
545-PPT-7* |
Z40,670-8 |
| 8 |
13/6 |
535-PP-8 |
Z27,455-0 |
| 9 |
13/6 |
535-PP-9 |
Z27,456-9 |
| 800 MHz tubes |
| 7 |
3.8/3.8 |
541-PP-7 |
Z41,200-7 |
| 8 |
3.8/3.8 |
541-PP-8 |
Z41,201-5 |
| 900 MHz tubes |
| 7 |
2.5/3.8 |
542-PP-7 |
Z41,202-3 |
| 8 |
2.5/3.8 |
542-PP-8 |
Z41,203-1 |
* Ultra thin wall (0.09in.)
** Medium wall (0.03in.) |
|
TOP
10mm NMR tubes — 0.018in. wall thickness (Pkg=5 tubes) |
| L(in.) |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 60MHz tubes |
| 7 |
NA |
513-1PS-7 |
Z27,477-1 |
| 8 |
NA |
513-1PS-8 |
Z27,479-8 |
| 9 |
NA |
513-1PS-9 |
Z27,480-1 |
| 100MHz tubes |
| 7 |
254/51 |
Z27,468-2 |
Z27,203-5 |
| 8 |
254/51 |
513-1PP-8 |
Z27,469-0 |
| 9 |
254/51 |
513-1PP-9 |
Z27,470-4 |
| 300MHz tubes |
| 7 |
76/38 |
513-3PP-7 |
Z27,203-5 |
| 8 |
76/38 |
513-3PP-8 |
Z27,471-2 |
| 9 |
76/38 |
513-3PP-9 |
Z27,204-3 |
| 360MHz tubes |
| 7 |
51/25 |
513-5PP-7 |
Z27,472-0 |
| 8 |
51/25 |
513-5PP-8 |
Z27,473-9 |
| 9 |
51/25 |
513-5PP-9 |
Z27,474-7 |
| 400MHz tubes |
| 7 |
38/13 |
513-7PP-7 |
Z27,205-1 |
| 8 |
38/13 |
513-7PP-8 |
Z27,475-5 |
| 9 |
38/13 |
513-7PP-9 |
Z27,476-3 |
| *Tubes do not have a precision i.d. tolerance. |
TOP
Wilmad Screw Cap NMR Tubes
NMR tube has an open-top, screw-thread cap with a PTFE/silicone septum that permits addition of reactants or samples via syringe through the cap. Also good for sample storage. Caps and septa are replaceable. Excellent for handling air-sensitive samples and in cell perfusion studies. Tubes are 7in. L.
 |
| 5mm NMR tubes (Pkg=1 tube) |
| Product Name |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 100MHz tube |
76/51 |
505-TR-7 |
Z27,191-8 |
| 100MHz tube |
51/51 |
506-TR-7 |
Z27,192-6 |
| 360MHz tube |
51/25 |
507-TR-7 |
Z27,193-4 |
| 400MHz tube |
25/13 |
528-TR-7 |
Z27,194-2 |
| 360MHz tube |
51/25 |
507-TR-7 |
Z27,193-4 |
| 400MHz tube |
25/13 |
528-TR-7 |
Z27,194-2 |
| 500MHz tube |
13/60 |
535-TR-7 |
Z27,195-0 |
|
8mm NMR tubes (Pkg=1 tube) |
| Product Name |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 400MHz tube |
38/13 |
513A-7TR |
Z27,482-8 |
|
10mm NMR tubes (Pkg=1 tube) |
| Product Name |
Concentricity/camber (µm) |
Wilmad No. |
Cat. No. |
| 300MHz tube |
76/38 |
513-3TRA-7 |
Z27,196-9 |
| 400MHz tube |
38/13 |
513-7TRA-7 |
Z27,197-7 |
| Replacement caps and septa for screw-cap NMR tubes
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TOP |
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