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GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-TA

GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-TA

Conditions

column Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 µm (73023AST)
carrier gas helium, 30 psi
gradient 80 C, 2 C/min to 110 C
sample 2.5 mg/mL each racemate in methanol (N-TFA derivatives)
injection 0.6 µL, 80:1 split
inj. temp. 250 C
detector FID, 250 C

Description

Categories Analytical Chromatography, GC Applications, Enantiomers, Amines
Featured Industry Chemicals and Industrial Polymers
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CHIRALDEX is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Materials

     
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