GC Analysis of Amphetamine and Methamphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® G-PN

GC Analysis of Amphetamine and Methamphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® G-PN

Conditions

column Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 µm (74033AST)
oven 130 C
carrier gas helium, 30 psi
sample 3 mg/mL each compound in methanolpeak 1: d-methamphetaminepeak 2: l-methamphetaminepeak 3: l-amphetaminepeak 4: d-amphetamine
injection 1 µL, 80:1 split
inj. temp. 250 C
detector FID, 250 C

Description

Analysis Note Elution order reversal of amphetamine (d,l) by using CHIRALDEX G-DP, 140°C.
Categories Analytical Chromatography, Chiral Applications, GC Applications, Clinical, Forensic & Toxicology, Enantiomers, Pharmaceuticals, Drugs of Abuse, Amines
Featured Industry Clinical
Forensics and Toxicology
Pharmaceutical (small molecule)
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CHIRALDEX is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Materials

     
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