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GC Analysis of Basic Drugs on SLB®-5ms

GC Analysis of Basic Drugs on SLB®-5ms

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.50 µm (28473-U)
oven 45 C (2.0 min), 30 C/min to 110 C (1.0 min), 15 C/min to 200 C (1.0 min), 4 C/min to 310 C (5.0 min)
carrier gas helium, 0.7 ml/min constant
sample drugs of abuse standard diluted to 100 ppm in methanol
injection 0.5 µL, pulsed splitless, 30 psi (0.20 min), purge on (1.50 min), purge flow (50.0 ml/min)
liner 2 mm I.D., straight
inj. temp. 250 C
MSD interface 330 C
scan range m/z = 40-450

Description

Categories Analytical Chromatography, GC Applications, Drugs of Abuse, Pharmaceuticals
Featured Industry Forensics and Toxicology
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • Amitriptyline
  • Caffeine
  • Cocaine
  • Codeine
  • Desipramine
  • Diazepam
  • Diphenhydramine
  • Fentanyl
  • Heroin
  • Lidocaine
  • Methamphetamine
  • Methodone
  • Morphine
  • Nicotine
  • Phenobarbital
  • Prazepam

Materials

     
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