GC Analysis of Fragrance Compounds in Shampoo Base on a 100% Methyl Column after SPME using 100 μm PDMS Fiber

GC Analysis of Fragrance Compounds in Shampoo Base on a 100% Methyl Column after SPME using 100 μm PDMS Fiber

Conditions

desorption process 5 min, 250 C
desorption temp. -50 C w/liquid CO2
extraction headspace, 5 min, 80 C (with sample stirring)
SPME fiber polydimethylsiloxane, 100 µm film (57300-U)
column 100% methyl polysiloxane, 50 m x 0.25 mm I.D., 0.25 µm (Supelco equivalent, Equity-1, 28047-U)
oven 35 C to 240 C at 3 C/min
carrier gas helium, 0.5 ml/min
sample 0.5 g shampoo base with 1% fragrance test mix, diluted 1:1 with NaCl/water in a 10 mL vial
inj. temp. split, 250 C
detector MSD, scan m/z = 29-350 AMU

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Foods, Flavors & Fragrances, Volatiles
Featured Industry Cosmetics, Personal Care, and Cleaning Products
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for SPME, application for GC

Analyte

  • (±)-Citronellal
  • (R)-(+)-Limonene
  • Benzyl acetate
  • Benzyl salicylate
  • Citronellol
  • Eugenol
  • Heliotropine
  • Linalool
  • Linalyl acetate
  • Menthol
  • Methyl ionone gamma
  • Methyl salicylate
  • Myrcene
  • α-Hexylcinnamaldehyde
  • α-Terpineol

Materials

     
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