GC Analysis of Residual Solvents on SPB®-624 after SPME using 100 μm PDMS Fiber

GC Analysis of Residual Solvents on SPB®-624 after SPME using 100 μm PDMS Fiber

Conditions

extraction headspace or immersion sampling (15 min) 1 min desorption
SPME fiber polydimethylsiloxane, 100 µm (57300-U)
column SPB-624, 75 m x 0.53 mm I.D., 3.0 µm (25432)
oven 40 °C (35 min) to 220 °C at 40 °C/min, hold 5 min
carrier gas helium, 35 cm/sec
inj. temp. splitless (closed 3 min), 200 °C
detector FID, 250 °C

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Solvents
Featured Industry Pharmaceutical (small molecule)
Legal Information SPB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for SPME, application for GC

Analyte

  • 1,4-Dioxane
  • Acetone
  • Benzene
  • Chloroform
  • Ethanol
  • Isopropanalol
  • Methanol
  • Methylene chloride
  • Trichloroethylene

Materials

     
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