US EPA Method 1668: GC Analysis of PCB Congeners (18-Component Toxic Congener Mix) on SPB®-Octyl

US EPA Method 1668: GC Analysis of PCB Congeners (18-Component Toxic Congener Mix) on SPB®-Octyl

Conditions

column SPB-Octyl, 60 m x 0.25 mm I.D., 0.25 µm (24219-U)
oven 150 °C (4 min), 6 C/min to 320 °C (16 min)
carrier gas helium, 20 cm/sec at 200 °C
sample PCB mixture in isooctane, each analyte at 50-200 ng/mL
injection 1 µL, splitless (45 sec)
inj. temp. 250 °C
detector ECD, 340 °C

Description

Categories Analytical Chromatography, GC Applications, Dioxins/PCBs/PBDEs
Featured Industry Environmental
Legal Information SPB is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Materials

     
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