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US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms

US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 45 C (1 min), 50 C/min to 130 C (1 min), 12 C/min to 180 C, 7 C/min to 240 C, 12 C/min to 330 C (2 min)
carrier gas helium, 0.9 ml/min., constant flow
sample 2 ppm, in ethyl acetate, of a 102 component semivolatile standard plus 3 surrogate and 3 internal standard compounds (at 5 ppm)
injection 1 µl pulsed splitless (15 psi until 0.20 min) (1.0 min)
liner 4 mm I.D., single taper
inj. temp. 275 C
MSD interface 330 C
scan range m/z = 45-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Food and Beverages
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,1,1-Trichloro-2,2-bis(4-chlorophenyl)ethane (4,4′-DDT)
  • 1,1-Dichloro-2,2-bis(4-chlorophenyl)ethane (4,4′-DDD)
  • 1,3-Dimethyl-2-nitrobenzene
  • 2,2′,3,3′,4,4′,6-Heptachlorobiphenyl
  • 2,2′,3,3′,4,5′,6,6′-Octachlorobiphenyl
  • 2,2′,3′,4,6-Pentachlorobiphenyl
  • 2,2′,4,4′,5,6′-Hexachlorobiphenyl
  • 2,2′,4,4′-Tetrachlorobiphenyl
  • 2,3-Dichlorobiphenyl
  • 2,4′,5-Trichlorobiphenyl
  • 2,4-Dinitrotoluene
  • 2,6-Dinitrotoluene
  • 2-Chlorobiphenyl
  • 4,4′-DDE (1,1-Dichloro-2,2-bis(p-chlorophenyl)ethylene)
  • Acenaphthene-d10
  • Acenaphthylene
  • Alachlor
  • Aldrin
  • Ametryn
  • Anthracene
  • Atraton
  • Atrazine
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Bis(2-ethylhexyl) adipate
  • Bis(2-ethylhexyl) phthalate
  • Bromacil
  • Butachlor
  • Butylate
  • Butylbenzylphthalate
  • Carboxin
  • Chlomeb
  • Chlorobenzilate
  • Chloropryifos
  • Chlorothalonil
  • Chlorpropham
  • Chrysene
  • Chrysene-d12
  • Cyanazine
  • Cycloate
  • Dachal
  • Diazinon
  • Dibenzo[a,h]anthracene
  • Dichlorvos
  • Dieldrin
  • Diethyl phthalate
  • Dimethylphthalate
  • Di-n-Butyl phthalate
  • Diphenamid
  • Disulfoton
  • Endosulfan I
  • Endosulfan II
  • Endosulfan sulfate
  • Endrin
  • Endrin aldehyde
  • Endrin ketone
  • Ethoprop
  • Etridiazole
  • Fenamiphos
  • Fenarimol
  • Fluorene
  • Heptachlor
  • Heptachlor epoxide
  • Hexachlorobenzene
  • Hexachlorocyclopentadiene
  • Hexazinone
  • Indeno[1,2,3-cd]pyrene
  • Isophorone
  • Methoxychlor
  • Methyl paraxon
  • Metolachlor
  • Metribuzin
  • Mevinphos
  • Molinate
  • Napropamide
  • N-Octyl bicycloheptene dicarboximide (MGK 264)
  • Norflurazon
  • Pebulat
  • Pentachlorophenol
  • Permethrin
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d12
  • Prometon
  • Prometryn
  • Pronamide
  • Propachlor
  • Propazine
  • Pyrene
  • S-Ethyl dipropyl(thiocarbamate) (EPTC)
  • Simetryn
  • Stirofos (Tetrachlorvinphos)
  • Tebuthiuron
  • Terbacil
  • Terbufos
  • Terbutryn
  • Triadimefon
  • Trifluralin
  • Triphenyl phosphate
  • Vernclate
  • α-BHC
  • α-Chlordane
  • β-BHC
  • γ-Chlordane
  • δ-BHC

Materials

     
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