US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SPB®-608

US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SPB®-608

Conditions

column SPB-608, 30 m x 0.25 mm I.D., 0.25 µm (24103-U)
oven 75 °C (2 min), 15 °C/min to 300 °C (5 min)
carrier gas helium, 1.2 mL/min. constant
sample mixture of 608.1 and 608.2 calibration solutions (40351-U and 40352-U) diluted to 100 ppb in n-hexane
injection 1 µL, splitless (splitter open after 0.75 min)
liner 4 mm I.D., single taper
inj. temp. 250 °C
detector ECD, 300 °C

Description

Categories Analytical Chromatography, GC Applications, Pesticides
Featured Industry Environmental
Legal Information SPB is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Materials

     
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