US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 40 C (2 min), 22 C/min to 240 C, 10 C/min to 330 C, (1 min)
carrier gas helium, 1.0 ml/min (11 min), 10 ml/min to 1.5 ml/min (hold remainder of run)
sample 50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column)
injection 0.5 µL, splitless (0.50 min)
liner 2 mm I.D., straight
inj. temp. 250 C
MSD interface 330 C
scan range m/z = 40-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,2,4-Trichlorobenzene
  • 1,2-Dichlorobenzene
  • 1,2-Dichlorobenzene-d4
  • 1,3-Dichlorobenzene
  • 1,4-Dichlorobenzene
  • 1,4-Dichlorobenzene-d4
  • 2,4,5-Trichlorophenol
  • 2,4,6-Tribromophenol
  • 2,4,6-Trichlorophenol
  • 2,4-Dichlorophenol
  • 2,4-Dimethylphenol
  • 2,4-Dinitrophenol
  • 2,4-Dinitrotoluene
  • 2,6-Dinitrotoluene
  • 2-Chloronaphthalene
  • 2-Chlorophenol
  • 2-Chlorophenol-d4
  • 2-Fluorobiphenyl
  • 2-Fluorophenol
  • 2-Methyl-4,6-dinitrophenol
  • 2-Methylnaphthalene
  • 2-Methylphenol
  • 2-Nitroaniline
  • 2-Nitrophenol
  • 3,3′-Dichlorobenzidine
  • 3,3′-Dimethylbenzidine
  • 3-Nitroaniline
  • 4-Bromophenyl phenyl ether
  • 4-Chloro-3-methylphenol
  • 4-Chloroaniline
  • 4-Chlorophenylphenyl ether
  • 4-Methylphenol
  • 4-Nitroaniline
  • 4-Nitrophenol
  • Acenaphthene
  • Acenaphthene-d10
  • Acenaphthylene
  • Aniline
  • Anthracene
  • Azobenzene
  • Benzidine
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Benzoic acid
  • Benzyl alcohol
  • Bis(2-chloroethoxy)methane
  • Bis(2-chloroethyl) ether
  • Bis(2-chloroisopropyl) ether
  • Bis(2-ethylhexyl) phthalate
  • Butylbenzylphthalate
  • Carbazole
  • Chrysene
  • Chrysene-d12
  • Dibenzo[a,h]anthracene
  • Dibenzofuran
  • Diethyl phthalate
  • Dimethylphthalate
  • Di-n-Butyl phthalate
  • Di-n-Octyl phthalate
  • Fluoranthene
  • Fluorene
  • Hexachlorobenzene
  • Hexachlorobutadiene
  • Hexachlorocyclopentadiene
  • Hexachloroethane
  • Indeno[1,2,3-cd]pyrene
  • Isophorone
  • Naphthalene
  • Naphthalene-d2
  • Nitrobenzene
  • Nitrobenzene-d5
  • N-Nitrosodimethylamine
  • N-Nitroso-di-n-propylamine
  • N-Nitrosodiphenylamine
  • Pentachlorophenol
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d12
  • Phenol
  • Phenol-d6
  • Pyrene
  • Pyridine
  • Terphenyl-d14

Materials

     
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