US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm), 28 °C/min Oven Ramp, Fast GC Analysis

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm), 28 °C/min Oven Ramp, Fast GC Analysis

Conditions

column SLB-5ms, 20 m x 0.18 mm I.D., 0.36 µm (28576-U)
oven 50 °C (0.50 min), 28 °C/min to 250 °C, 35 °C/min to 340 °C (5 min)
carrier gas helium, 1.4 mL/min constant
sample 80 °Component semivolatile standard at 50 ppm, plus 6 internal standards (at 40 ppm) in methylene chloride
injection 0.50 µL, reduced pressure to 20 psi at injection (0.1 min) (splitter open at 0.75 min)
liner 2 mm I.D., straight
inj. temp. 250 °C
MSD interface 340 °C
scan range m/z = 40-450

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 1,2,4-Trichlorobenzene
  • 1,2-Dichlorobenzene
  • 1,2-Dichlorobenzene-d4
  • 1,3-Dichlorobenzene
  • 1,4-Dichlorobenzene
  • 1,4-Dichlorobenzene-d4
  • 2,4,5-Trichlorophenol
  • 2,4,6-Tribromophenol
  • 2,4,6-Trichlorophenol
  • 2,4-Dichlorophenol
  • 2,4-Dimethylphenol
  • 2,4-Dinitrophenol
  • 2,4-Dinitrotoluene
  • 2,6-Dinitrotoluene
  • 2-Chloronaphthalene
  • 2-Chlorophenol
  • 2-Chlorophenol-3,4,5,6-d4
  • 2-Fluorobiphenyl
  • 2-Fluorophenol
  • 2-Methyl-4,6-Dinitrophenol
  • 2-Methylnaphthalene
  • 2-Nitroaniline
  • 2-Nitrophenol
  • 3,3′-Dichlorobenzidine
  • 3-Nitroaniline
  • 4-Bromodiphenyl ether
  • 4-Chloro-3-methylphenol
  • 4-Chloroaniline
  • 4-Chlorodiphenyl ether
  • 4-Nitroaniline
  • 4-Nitrophenol
  • Acenaphthene
  • Acenaphthene-d10
  • Acenaphthylene
  • Aniline
  • Anthracene
  • Azobenzene
  • Benzidine
  • Benzo[a]anthracene
  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Benzoic acid
  • Benzyl alcohol
  • Benzylbutylphthalate
  • Bis(2-chloroethoxy)methane
  • Bis(2-chloroethyl) ether
  • Bis(2-chloroisopropyl) ether
  • Bis(2-ethylhexyl) phthalate
  • Carbazole
  • Chrysene
  • Chrysene-d12
  • Dibenzo[a,h]anthracene
  • Dibenzofuran
  • Dibutyl phthalate
  • Diethyl phthalate
  • Dimethylphthalate
  • Di-n-Octyl phthalate
  • Fluoranthene
  • Fluorene
  • Hexachloro-1,3-Butadiene
  • Hexachlorobenzene
  • Hexachlorocyclopentadiene
  • Hexachloroethane
  • Indeno[1,2,3-cd]pyrene
  • Isophorone
  • Naphthalene
  • Naphthalene-d8
  • Nitrobenzene
  • Nitrobenzene-d5
  • N-Nitrosodimethylamine
  • N-Nitroso-di-n-propylamine
  • N-Nitrosodiphenylamine
  • o-Toluidine
  • p-Cresol
  • Pentachlorophenol
  • Perylene-d12
  • Phenanthrene
  • Phenanthrene-d10
  • Phenol
  • Phenol-d6
  • p-Terphenyl-d14
  • Pyrene
  • Pyridine
  • α-Cresol

Materials

     
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