US EPA Method TO-17: GC Analysis of Volatiles on Equity®-1 after Collection/Desorption using Carbotrap 300 Tube

US EPA Method TO-17: GC Analysis of Volatiles on Equity®-1 after Collection/Desorption using Carbotrap 300 Tube

Conditions

sample/matrix TO15/17 °Calibration Mix, 1 PPM in N2 (41973-U)
dry purge 1 min
thermal desorption tube Carbotrap® 300 glass TD tube, fritted, O.D. x L 1/4 in. x 3 1/2 in., unconditioned, pkg of 10 ea (30141-U)
bake 350 °C
column FS CAP Equity-1 30 m x 0.25 mm I.D. x 1.0 µm (28049-U)
oven 40 °C/8 min to 100 °C @ 5 °C/min to 220 °C @ 15 °C/min, hold for 10 min
carrier gas Helium
transfer line/valve temp. 175 °C
detector MSD
MSD interface 175 °C
scan range 35-265

Description

Analysis Note This application shows the chromatography achieved using an Equity-1 column.
Categories Analytical Chromatography, GC Applications, Volatiles
Featured Industry Environmental
Industrial Hygiene
Legal Information Carbotrap is a registered trademark of Sigma-Aldrich Co. LLC, Equity is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Analyte

  • 1,1,1-Trichloroethane
  • 1,1,2,2-Tetrachloroethane
  • 1,1,2-Trichloroethane
  • 1,1,2-Trichlorotrifluoroethane
  • 1,1-Dichloroethane
  • 1,1-Dichloroethylene
  • 1,2,4-Trichlorobenzene
  • 1,2,4-Trimethylbenzene
  • 1,2-Dibromoethane
  • 1,2-Dichlorobenzene
  • 1,2-Dichloroethane
  • 1,2-Dichloropropane
  • 1,2-Dichlorotetrafluoroethane
  • 1,3,5-Trimethylbenzene
  • 1,3-Butadiene
  • 1,3-Dichlorobenzene
  • 1,4-Dichlorobenzene
  • 1,4-Dioxane
  • 1-Ethyl-4-methylbenzene
  • 2-Butanone
  • Acetone
  • Benzene
  • Benzyl chloride
  • Bromodichloromethane
  • Carbon disulfide
  • Carbon tetrachloride
  • Chlorobenzene
  • Chloroform
  • cis-1,2-Dichloroethylene
  • cis-1,3-Dichloropropene
  • Cyclohexane
  • Dibromochloromethane
  • Ethanol
  • Ethyl acetate
  • Ethyl chloride
  • Ethylbenzene
  • Hexachloro-1,3-butadiene
  • Isopropyl alcohol
  • Methyl isobutyl ketone
  • Methyl N-butyl ketone
  • Methylene chloride
  • m-Xylene
  • n-Heptane
  • n-Hexane
  • o-Xylene
  • p-Xylene
  • Styrene
  • tert-Butyl methyl ether
  • Tetrachloroethylene
  • Tetrahydrofuran (THF)
  • Toluene
  • trans-1,2-Dichloroethylene
  • trans-1,3-Dichloropropene
  • Tribromomethane
  • Trichloroethylene
  • Trichlorofluoromethane

Materials

     
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