US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food (Spiked) on SLB®-5ms

US FDA LIB 4423: GC Analysis of Melamine and Related Compounds in Dog Food (Spiked) on SLB®-5ms

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 115 C (3 min), 10 C/min to 325 C (6 min)
carrier gas helium, 1 ml/min., constant
sample TMS derivatives of melamine and related compounds (extract of dog food spiked with each analyte at 10 µg/g, with I.S. added at 1000 ng/mL, in pyridine:sylon BFT)
injection 1 muLsplitless
liner 4 mm I.D. single taper
inj. temp. 250 C
MSD interface 325 C
scan range SIM

Description

Categories Analytical Chromatography, GC Applications, Amines
Featured Industry Food and Beverages
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • 2,6-Diamino-4-chloropyrimidine
  • Ammelide
  • Ammeline
  • Cyanuric acid
  • Melamine

Materials

     
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