HPLC Analysis of 3,5-tBu-MeOBIPHEP Enantiomers on Astec® CHIROBIOTIC® V

HPLC Analysis of 3,5-tBu-MeOBIPHEP Enantiomers on Astec® CHIROBIOTIC® V

Conditions

column CHIROBIOTIC V, 25 cm x 4.6 mm I.D., 5 µm particles (11024AST)
column temp. 18 °C
mobile phase [A] n-hexane; [B] 10% ethanol in n-hexane; (75:25, A:B)
flow rate 1 mL/min
sample 3,5-tBu-MeOBIPHEP ((6,6′-dimethoxybiphenyl-2,2′-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine]), 1 mg/mL in ethanol with 5 drops of H2O2 added for oxidation
detector UV, 230 nm

Description

Categories Analytical Chromatography, Chiral Applications, Organic Chemicals, Catalysts, Chemicals and Industrial Polymers
Featured Industry Chemicals and Industrial Polymers
Legal Information CHIROBIOTIC is a registered trademark of Sigma-Aldrich Co. LLC, Astec is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for HPLC

Materials

     
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