Analytical Method: Iron in pickling baths

Instruments and Reagents:

Cat.No. 173016  Spectroquant® VIS Spectrophotometer Prove 100 or

Cat.No. 173017  Spectroquant® UV/VIS Spectrophotometer Prove 300 or

Cat.No. 173018  Spectroquant® UV/VIS Spectrophotometer Prove 600 or

Cat.No. 109748  Spectroquant® Photometer NOVA 30 or

Cat.No. 109751  Spectroquant® Photometer NOVA 60

Cat.No. 114946  Rectangular cells 10 mm and/or

Cat.No. 114947  Rectangular cells 20 mm and/or

Cat.No. 114944  Rectangular cells 50 mm
Cat.No. 114896  Spectroquant® Iron Cell Test
Cat.No. 116754  Water for analysis
 
As a rule the iron in these situation is in ionic form, therefore a special prior decomposition is not necessary.
 
Sample preparation:
In a 1000-ml volumetric flask place 10 ml of the filtered test solution, fill up to the mark with water for analysis and mix well. Place 10 ml of this solution in a 1000-ml volumetric flask and fill up to volume with water for analysis. The total dilution is 1:10000.
 
Analysis:
Determine with the above mentioned test kit.
 
Calculation:
Iron content in g/l Fe = analysis value in mg/l Fe x 10

Materials

     
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