GC Analysis / Mass Spectrum of Benzo[g,h,i]Perylene (elutes at 325 °C) on SLB®-5ms, from US EPA Method 8270

GC Analysis / Mass Spectrum of Benzo[g,h,i]Perylene (elutes at 325 °C) on SLB®-5ms, from US EPA Method 8270

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 40 °C (3 min), 20 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (5 min)
carrier gas helium, pressure programmed, 20 psi (0 min), 99 psi/min to 80 psi (0 min), 99 psi/min to 16.5 psi (3 min), 99 psi/min to 25 psi (hold remainder of run)
sample 50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column)
injection 1.0 µL, splitless (0.75 min)
liner 4 mm I.D., single taper
inj. temp. 250 °C
MSD interface 325 °C
scan range 40-450 amu

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Analyte

  • Benzo[g,h,i]perylene

Materials

     
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