GC Analysis of 1-Phenylethylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-PH

GC Analysis of 1-Phenylethylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-PH

Conditions

column Astec CHIRALDEX B-PH, 30 m x 0.25 mm I.D., 0.12 µm (71023AST)
oven 120 °C
carrier gas helium, 30 psi
sample 3 mg/mL in methylene chloridepeak 1: S(-)-1-phenylethylamine (N-TFA derivative)peak 2: R(+)-1-phenylethylamine (N-TFA derivative)
inj. temp. 250 °C
detector FID, 250 °C

Description

Analysis Note Can reverse elution order by using CHIRALDEX G-PN, or by using the N-TFA derivative on the B-DM column.
Categories Analytical Chromatography, GC Applications, Anilines, Amines, Enantiomers
Featured Industry Chemicals and Industrial Polymers
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CHIRALDEX is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Materials

     
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