GC Analysis of a 19-Component PCB Congener Mix on SLB®-IL82

GC Analysis of a 19-Component PCB Congener Mix on SLB®-IL82

Conditions

column SLB-IL82, 30 m x 0.25 mm I.D., 0.20 µm (29479-U)
oven 50 ºC (2 min), 5 ºC/min to 260 ºC
carrier gas helium, 1.0 ml/min
sample PCB congener mix, each analyte at 2.5 ppm in n-hexane
injection 1 muLsplitless (splitter open at 1 min)
liner 4 mm I.D., split/splitless type, single taper design
inj. temp. 250 C
detector MSD, m/z = 100-550

Description

Categories Analytical Chromatography, GC Applications, Dioxins/PCBs/PBDEs
Featured Industry Environmental
Food and Beverages
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Analyte

  • 2,2’,3,3’,4,4’,5,5’,6-Nonachlorobiphenyl
  • 2,2’,3,3’,4,4’,5,5’-Octachlorobiphenyl
  • 2,2’,3,3’,4,5,5’,6,6’-Nonachlorobiphenyl
  • 2,2’,3,3’,5,5’,6,6’-Octachlorobiphenyl
  • 2,2’,3,4’,5,6,6’-Heptachlorobiphenyl
  • 2,2’,4,4’,6,6’-Hexachlorobiphenyl
  • 2,2’,4,6,6’-Pentachlorobiphenyl
  • 2,2’,6,6’-Tetrachlorobiphenyl
  • 2,4,6-Trichlorobiphenyl
  • 2,6-Dichlorobiphenyl
  • 2-Monochlorobiphenyl
  • 3,3’,4,4’,5,5’-Hexachlorobiphenyl
  • 3,3’,4,4’,5-Pentachlorobiphenyl
  • 3,3’,4,4’-Tetrachlorobiphenyl
  • 3,4,4’-Trichlorobiphenyl
  • 4,4’-Dichlorobiphenyl
  • 4-Monochlorobiphenyl
  • Biphenyl
  • Decachlorobiphenyl

Materials

     
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