GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-TA

GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX® B-TA

Conditions

column Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 µm (73023AST)
carrier gas helium, 30 psi
gradient 80 °C, 2 °C/min to 110 °C
sample 2.5 mg/mL each racemate in methanol (N-TFA derivatives)
injection 0.6 µL, 80:1 split
inj. temp. 250 °C
detector FID, 250 °C

Description

Categories Analytical Chromatography, GC Applications, Enantiomers, Amines
Featured Industry Chemicals and Industrial Polymers
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CHIRALDEX is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Materials

     
Related Links