GC Analysis of Basic Drugs on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after SPME using 85 μm Polyacrylate Fiber, Fast GC Analysis

GC Analysis of Basic Drugs on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after SPME using 85 μm Polyacrylate Fiber, Fast GC Analysis

Conditions

sample/matrix 500 µg/L of each compound in 2 mL 0.05M phosphate buffer, pH=11, plus sodium chloride (NaCl) to 25% (w/v)
desorption process 250 °C for 3 min
extraction immersion, 450 rpm stirring at room temp. for 15 min
SPME fiber 85 µm Polyacrylate (57304)
column SLB-5ms, 20 m x 0.18 mm I.D. x 0.36 µm (28576-U)
oven 100 °C (1 min), 20 °C/min to 325 °C (5 min)
carrier gas helium, 1.5 mL/min. constant
liner 0.75 mm I.D. SPME
MSD interface 325 °C

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Drugs & Pharmaceuticals, Pharmaceuticals, Drugs of Abuse
Featured Industry Forensics and Toxicology
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for SPME, application for GC

Materials

     
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