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GC Analysis of Blood Alcohols in Human Plasma on SUPELCOWAX® 10 after SPME using 60 μm Carbowax® Fiber

GC Analysis of Blood Alcohols in Human Plasma on SUPELCOWAX® 10 after SPME using 60 μm Carbowax® Fiber

Conditions

sample/matrix blood alcohols at concentrations indicated in human plasma
desorption process 220 C, 2 min
extraction headspace, 50 C (5 min)
SPME fiber 60 µm Carbowax
column SUPELCOWAX 10, 30 m x 0.25 mm I.D., 0.50 µm (24284)
oven 35 C (2 min), 10 C/min to 125 C (1 min)
carrier gas helium, 1.0 ml/min constant
injection 10:1 split
liner 0.75 mm I.D. SPME liner
detector FID, 200 C

Description

Categories Analytical Chromatography, SPME Applications, GC Applications, Clinical, Forensic, Bioanalytical, Drugs & Pharmaceuticals, Drugs of Abuse, Alcohols
Featured Industry Forensics and Toxicology
Legal Information SUPELCOWAX is a registered trademark of Sigma-Aldrich Co. LLC, Carbowax is a registered trademark of Union Carbide
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for SPME, application for GC

Analyte

  • 1-Propanol
  • 2-Butanol
  • 2-Butanol
  • Acetaldehyde
  • Acetone
  • Ethanol
  • Methanol

Materials

     
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