GC Analysis of Class 3 Residual Solvents on SUPELCOWAX® 10

GC Analysis of Class 3 Residual Solvents on SUPELCOWAX® 10

Conditions

column SUPELCOWAX 10, 30 m x 0.53 mm I.D., 1.0 µm (25301-U)
oven 35 C (15 min), 5 C/min to 200 C
carrier gas helium, 30 cm/sec @ 35 C
sample 27 analytes, each at 3000 µg/mL in methanol
injection 1.0 muL33:1 split
liner single taper
inj. temp. 225 C
detector FID, 250 C

Description

Categories Analytical Chromatography, GC Applications, Solvents
Featured Industry Pharmaceutical (small molecule)
Legal Information SUPELCOWAX is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Analyte

  • 1-Butanol
  • 1-Propanol
  • 2-Butanone
  • 2-Propanol
  • 4-Methyl-2-pentanone
  • Acetic acid
  • Acetone
  • Anisole
  • Butyl acetate
  • Cumene
  • Diethyl ether
  • Dimethyl sulfoxide
  • Ethanol
  • Ethyl acetate
  • Ethyl formate
  • Heptane
  • Isoamyl alcohol
  • Isobutanol
  • Isobutyl acetate
  • Isopropyl acetate
  • Methyl acetate
  • Methyl-t-butyl ether
  • n-Amyl alcohol
  • Pentane
  • Propyl acetate
  • sec-Butanol
  • Tetrahydrofuran (THF)

Materials

     
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