GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (15 m x 0.10 mm I.D., 0.10 μm)

GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (15 m x 0.10 mm I.D., 0.10 μm)

Conditions

column SLB-5ms, 15 m x 0.10 mm I.D., 0.10 µm (28466-U)
oven 40 °C (2 min), 22 °C/min to 240 °C, 10 °C/min to 330 °C (1 min)
carrier gas helium, 30 cm/sec @ 200 °C, set using methane
sample 50 ng on-column of a 72 °Component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column), in methylene chloride
injection 0.1 µLsplitless (0.75 min)
liner 2 mm I.D., straight
inj. temp. 250 °C
detector FID, 330 °C

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Analyte

  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Indeno[1,2,3-cd]pyrene
  • Perylene-d12

Materials

     
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