GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (30 m x 0.25 mm I.D., 0.25 μm)

GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (30 m x 0.25 mm I.D., 0.25 μm)

Conditions

column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 40 C (2 min), 22 C/min to 240 C, 10 C/min to 330 C (1 min)
carrier gas helium, 30 cm/sec @ 200 C, set using methane
sample 50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column), in methylene chloride
injection 0.5 muLsplitless (0.75 min)
liner 4 mm I.D., single taper
inj. temp. 250 C
detector FID, 330 C

Description

Categories Analytical Chromatography, GC Applications, Semivolatiles
Featured Industry Environmental
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
Other Notes Complementary products:
Syringes
Vials
Gas Purification and Gas Management
Inlet Liners, Glass Wool, and Specialized Hand Tools
Septa and Specialized Hand Tools
Column Ferrules, Nuts, and Specialized Hand Tools
suitability application for GC

Analyte

  • Benzo[a]pyrene
  • Benzo[b]fluoranthene
  • Benzo[g,h,i]perylene
  • Benzo[k]fluoranthene
  • Indeno[1,2,3-cd]pyrene
  • Perylene-d12

Materials

     
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